Phenol, 2-(2-cyclohexen-1-yl)-6-methoxy-

Base Information

Chemical Name:Phenol, 2-(2-cyclohexen-1-yl)-6-methoxy-
CAS No.:69914-70-1
Molecular Formula:C13H16O2
Molecular Weight:204.269
Hs Code.:
DSSTox Substance ID:DTXSID50439967
Nikkaji Number:J494.642A

Synonyms:Phenol, 2-(2-cyclohexen-1-yl)-6-methoxy-;69914-70-1;DTXSID50439967;2-(2-Cyclohexenyl)-6-methoxyphenol

Suppliers and Price of Phenol, 2-(2-cyclohexen-1-yl)-6-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Phenol, 2-(2-cyclohexen-1-yl)-6-methoxy-

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:204.115029749
Heavy Atom Count:15
Complexity:225

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1O)C2CCCC=C2

Technology Process of Phenol, 2-(2-cyclohexen-1-yl)-6-methoxy-

There total 5 articles about Phenol, 2-(2-cyclohexen-1-yl)-6-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 145059-62-7
3-(cyclohex-2-en-1-yl)-1,2-dimethoxybenzene

: 69914-70-1
6-Methoxy-2-cycyclohexenyl-2-phenol

Guidance literature:: With trimethylsilyl iodide; In chloroform; for 1h; Ambient temperature;
DOI:10.1080/00397919208021674

Reference yield: 58.0%

: 90-05-1
2-methoxy-phenol

: 822-67-3
Cyclohex-2-enol

: 69914-70-1
6-Methoxy-2-cycyclohexenyl-2-phenol

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 220 ℃; for 0.5h; microwave irradiation;
DOI:10.1016/j.tetlet.2005.10.096

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 69914-70-1
6-Methoxy-2-cycyclohexenyl-2-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, 2.) I₂ / 1.) THF, hexane, from -10 deg C to RT, 2 h, 2.) THF, 20 deg C, 2 h

2: 50 percent / Pd(OAc)2, n-Bu₄NCl, KOAc, PPh₃ / dimethylformamide / 72 h / 80 °C

3: 65 percent / trimethylsilyl iodide / CHCl₃ / 1 h / Ambient temperature

With palladium diacetate; n-butyllithium; trimethylsilyl iodide; tetrabutyl-ammonium chloride; iodine; potassium acetate; triphenylphosphine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1080/00397919208021674