2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride

Base Information

Chemical Name:2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride
CAS No.:69920-06-5
Molecular Formula:C9H10ClNO6S
Molecular Weight:295.701
Hs Code.:
Mol file:69920-06-5.mol

Synonyms:2-(2-Methoxy-ethoxy)-5-nitro-benzenesulfonyl chloride;2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl Chloride;

Suppliers and Price of 2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride

Chemical Property:

Melting Point:73 - 74 °C
PSA：106.80000
LogP:3.15150

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride

There total 4 articles about 2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 69920-00-9
Sodium 2-(2-Methoxyethoxy)-5-nitrobenzenesulfonate

: 69920-06-5
2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride

Guidance literature:: With trichlorophosphate; In sulfolane; acetonitrile; at 68 - 72 ℃; for 0.666667h;
DOI:10.1055/s-1982-29823

Reference yield:

: 946-30-5
2-chloro-5-nitrobenzenesulphonic acid sodium salt

: 69920-06-5
2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / aq. NaOH, Na₂O*nSiO₂ / 3 h / 60 - 63 °C

2: 96 percent / POCl₃ / acetonitrile; tetrahydrothiophene 1,1-dioxide / 0.67 h / 68 - 72 °C

With sodium oxide; sodium hydroxide; trichlorophosphate; In sulfolane; acetonitrile;
DOI:10.1055/s-1982-29823