Benzene, [[(1-methyl-2-propynyl)oxy]methyl]-

Base Information

Chemical Name:Benzene, [[(1-methyl-2-propynyl)oxy]methyl]-
CAS No.:69939-72-6
Molecular Formula:C11H12O
Molecular Weight:160.216
Hs Code.:
DSSTox Substance ID:DTXSID60420129
Nikkaji Number:J1.327.454A

Synonyms:UPCMLD00WJLM61;69939-72-6;Benzene, [[(1-methyl-2-propynyl)oxy]methyl]-;3-(Benzyloxy)-1-butyne;DTXSID60420129

Suppliers and Price of Benzene, [[(1-methyl-2-propynyl)oxy]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzene, [[(1-methyl-2-propynyl)oxy]methyl]-

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:160.088815002
Heavy Atom Count:12
Complexity:159

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C#C)OCC1=CC=CC=C1

Technology Process of Benzene, [[(1-methyl-2-propynyl)oxy]methyl]-

There total 2 articles about Benzene, [[(1-methyl-2-propynyl)oxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100-39-0
benzyl bromide

: 2028-63-9
but-3-yn-2-ol

: 69939-72-6
[(but-3-yn-2-yloxy)methyl]benzene

Guidance literature:: but-3-yn-2-ol; With sodium hydride; In tetrahydrofuran; for 0.5h;

benzyl bromide; In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.1002/adsc.201701322

Reference yield:

: 100-44-7
benzyl chloride

: 69939-72-6
[(but-3-yn-2-yloxy)methyl]benzene

Guidance literature:: With potassium hydroxide;

Reference yield: 95.0%

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 69939-72-6
[(but-3-yn-2-yloxy)methyl]benzene

: 2-benzyloxy-9-hydroxy-non-3-yn-5-one

Guidance literature:: [(but-3-yn-2-yloxy)methyl]benzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.333333h;

With boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 ℃; for 0.166667h;

3,4,5,6-tetrahydro-2H-pyran-2-one; In tetrahydrofuran; at -78 - 20 ℃; for 1h;