Methyl 2-[(triphenyl-lambda~5~-phosphanylidene)amino]benzoate

Base Information

Chemical Name:Methyl 2-[(triphenyl-lambda~5~-phosphanylidene)amino]benzoate
CAS No.:70036-31-6
Molecular Formula:C₂₆H₂₂NO₂P
Molecular Weight:411.44
Hs Code.:
DSSTox Substance ID:DTXSID70579899
Nikkaji Number:J452.160I
Wikidata:Q82470552

Synonyms:70036-31-6;SCHEMBL14010928;DTXSID70579899;Methyl 2-[(triphenyl-lambda~5~-phosphanylidene)amino]benzoate;Methyl 2-((triphenylphosphoranylidene)amino)benzoate

Suppliers and Price of Methyl 2-[(triphenyl-lambda~5~-phosphanylidene)amino]benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Methyl 2-[(triphenyl-lambda~5~-phosphanylidene)amino]benzoate

Chemical Property:

XLogP3:6.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:411.13881594
Heavy Atom Count:30
Complexity:548

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C1=CC=CC=C1N=P(C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Methyl 2-[(triphenyl-lambda~5~-phosphanylidene)amino]benzoate

There total 1 articles about Methyl 2-[(triphenyl-lambda~5~-phosphanylidene)amino]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134-20-3
2-carbomethoxyaniline

: 603-35-0
triphenylphosphine

: 70036-31-6
methyl 2-<(triphenylphosphoranylidene)amino>benzoate

Guidance literature:: With bromine; triethylamine; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 5 min, 2.) 25 deg C, 4 h;
DOI:10.1002/jhet.5570280810

Reference yield: 64.0%

: 70036-31-6
methyl 2-<(triphenylphosphoranylidene)amino>benzoate

: 103-71-9
phenyl isocyanate

: 139308-41-1
N-phenyl-N'-(2-methoxycarbonylphenyl)carbodiimide

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 1h;
DOI:10.1002/jhet.5570280810

Reference yield:

: 70036-31-6
methyl 2-<(triphenylphosphoranylidene)amino>benzoate

: 4248-15-1
2-anilinoquinazolin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / tetrahydrofuran / 1 h / 25 °C

2: 76 percent / NH₃ / tetrahydrofuran / 2 h / 25 °C

With ammonia; In tetrahydrofuran;
DOI:10.1002/jhet.5570280810