2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide

Base Information

Chemical Name:2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide
CAS No.:64493-21-6
Molecular Formula:C53H72 N2 O12 . 2 I
Molecular Weight:1182.97
Hs Code.:
European Community (EC) Number:264-921-1

2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide

Synonyms:EINECS 264-921-1;64493-21-6;2,2'-((Pentane-1,5-diylbis(oxy))bis(3-oxopropane-3,1-diyl))bis(1-(3,4-dimethoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinolin-2-ium) iodide;2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide;2,2'-[1,5-pentanediylbis[oxy(3-oxo-3,1-propanediyl)]]bis[1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium] diiodide;C53H72N2O12.2I;C53-H72-N2-O12.2I

Suppliers and Price of 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:14
Rotatable Bond Count:26
Exact Mass:1182.31747
Heavy Atom Count:69
Complexity:1390

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+]1(CCC2=CC(=C(C=C2C1CC3=CC(=C(C=C3)OC)OC)OC)OC)CCC(=O)OCCCCCOC(=O)CC[N+]4(CCC5=CC(=C(C=C5C4CC6=CC(=C(C=C6)OC)OC)OC)OC)C.[I-].[I-]

Technology Process of 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide

There total 6 articles about 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 64228-78-0,64493-10-3,83285-74-9,96687-52-4,96687-53-5,110817-20-4
pentamethylene bis(1-(3,4-dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxy-1H-isoquinoline-2-propionate) dioxalate

: 74-88-4
methyl iodide

: 64493-21-6
C₅₃H₇₂N₂O₁₂⁽²⁺⁾*2I^(1-)

Guidance literature:: In acetonitrile; for 48h; Ambient temperature;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 64493-21-6
C₅₃H₇₂N₂O₁₂⁽²⁺⁾*2I^(1-)

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / 2 h / 190 - 210 °C

2: phosphoryl chloride / toluene / 3 h / Heating

3: 71 percent / sodium borohydride / 19 h / Ambient temperature

4: 51 percent / benzene / 48 h / Heating

5: 86 percent / acetonitrile / 48 h / Ambient temperature

With sodium tetrahydroborate; trichlorophosphate; In toluene; acetonitrile; benzene;

Reference yield:

: 139-76-4
N-(3,4-dimethoxyphenethyl)-2-(3,4-dimethoxyphenyl)acetamide

: 64493-21-6
C₅₃H₇₂N₂O₁₂⁽²⁺⁾*2I^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: phosphoryl chloride / toluene / 3 h / Heating

2: 71 percent / sodium borohydride / 19 h / Ambient temperature

3: 51 percent / benzene / 48 h / Heating

4: 86 percent / acetonitrile / 48 h / Ambient temperature

With sodium tetrahydroborate; trichlorophosphate; In toluene; acetonitrile; benzene;