1-Phenylhex-5-ene-1,4-dione

Base Information

Chemical Name:1-Phenylhex-5-ene-1,4-dione
CAS No.:70353-42-3
Molecular Formula:C12H12O2
Molecular Weight:188.226
Hs Code.:
DSSTox Substance ID:DTXSID60500430
Wikidata:Q82352009

Synonyms:1-Phenylhex-5-ene-1,4-dione;70353-42-3;SCHEMBL3628047;DTXSID60500430

Suppliers and Price of 1-Phenylhex-5-ene-1,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-Phenylhex-5-ene-1,4-dione

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:188.083729621
Heavy Atom Count:14
Complexity:225

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CC(=O)CCC(=O)C1=CC=CC=C1

Technology Process of 1-Phenylhex-5-ene-1,4-dione

There total 1 articles about 1-Phenylhex-5-ene-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 51171-73-4
4-hydroxy-4-phenylcyclohexanone

: 70353-42-3
1-phenyl-5-hexene-1,4-dione

Guidance literature:: With N-Bromosuccinimide; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; [bis(acetoxy)iodo]benzene; In tetrachloromethane; water; at 20 ℃; for 21h; Irradiation;
DOI:10.1039/C8SC01763H

Reference yield: 46.0%

: 70353-42-3
1-phenyl-5-hexene-1,4-dione

: 5453-80-5,19926-88-6,19926-90-0,58001-94-8,69831-12-5,69831-13-6,72203-35-1,96443-40-2,96443-41-3
bicyclo[2.2.1]hept-5-ene-2-carbaldehyde

: 79977-01-8,79977-44-9
1-(Bicyclo<2.2.1>hept-5-en-2-yl)-7-phenyl-1,4,7-heptantrion

Guidance literature:: With 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; triethylamine; at 65 ℃; for 15h;

Reference yield:

: 70353-42-3
1-phenyl-5-hexene-1,4-dione

: 79977-20-1
1-Phenyl-1,4,7,10-dodecantetraon

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazoliumchloride, triethylamine / 15 h / 65 °C

2: 85 percent / 500 °C / 10 Torr

3: 69 percent / 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazoliumchloride, triethylamine / ethanol / 15 h / 80 °C

With 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; triethylamine; In ethanol;