N,N-dimethyl-4-[5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl]aniline

Base Information

Chemical Name:N,N-dimethyl-4-[5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl]aniline
CAS No.:70366-88-0
Molecular Formula:C16H14N4O3
Molecular Weight:310.312
Hs Code.:
DSSTox Substance ID:DTXSID00364275
Wikidata:Q82148133

Synonyms:N,N-dimethyl-4-[5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl]aniline;70366-88-0;DTXSID00364275;STK041366;AKOS005383573;5-(4-dimethylaminophenyl)-2-(4-nitrophenyl)-1,3,4-oxadiazole

Suppliers and Price of N,N-dimethyl-4-[5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl]aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N-dimethyl-4-[5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl]aniline

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:310.10659032
Heavy Atom Count:23
Complexity:399

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC=C(C=C1)C2=NN=C(O2)C3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of N,N-dimethyl-4-[5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl]aniline

There total 4 articles about N,N-dimethyl-4-[5-(4-nitrophenyl)-1,3,4-oxadiazol-2-yl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: N-(4-dimethylaminobenzoyl)-N'-(4-nitrobenzoyl)hydrazine

: 70366-88-0
2-(4-nitrophenyl)-5-(4'-dimethylaminophenyl)-1,3,4-oxadiazole

Guidance literature:: With trichlorophosphate; for 6h; Reflux;
DOI:10.1016/j.dyepig.2017.09.010

Reference yield:

: 19353-92-5
4-(dimethylamino)benzohydrazide

: 70366-88-0
2-(4-nitrophenyl)-5-(4'-dimethylaminophenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / Heating

2: trichlorophosphate / 10 h / Reflux

With pyridine; trichlorophosphate;
DOI:10.1002/mrc.2804

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 70366-88-0
2-(4-nitrophenyl)-5-(4'-dimethylaminophenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1-methyl-pyrrolidin-2-one / 7 h / 0 - 20 °C

2: trichlorophosphate / 6 h / Reflux

With pyridine; trichlorophosphate; In 1-methyl-pyrrolidin-2-one;
DOI:10.1016/j.dyepig.2017.09.010