Benzamide, N-(2-amino-5-nitrophenyl)-4-nitro-

Base Information

Chemical Name:Benzamide, N-(2-amino-5-nitrophenyl)-4-nitro-
CAS No.:70499-97-7
Molecular Formula:C13H10N4O5
Molecular Weight:302.246
Hs Code.:
DSSTox Substance ID:DTXSID50389034

Synonyms:Benzamide, N-(2-amino-5-nitrophenyl)-4-nitro-;N-(2-amino-5-nitrophenyl)-4-nitrobenzamide;70499-97-7;N-(2-Amino-5-nitro-phenyl)-4-nitro-benzamide;SCHEMBL11346516;DTXSID50389034;AKOS000635202

Suppliers and Price of Benzamide, N-(2-amino-5-nitrophenyl)-4-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzamide, N-(2-amino-5-nitrophenyl)-4-nitro-

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:302.06511943
Heavy Atom Count:22
Complexity:439

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=O)NC2=C(C=CC(=C2)[N+](=O)[O-])N)[N+](=O)[O-]

Technology Process of Benzamide, N-(2-amino-5-nitrophenyl)-4-nitro-

There total 1 articles about Benzamide, N-(2-amino-5-nitrophenyl)-4-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 122-04-3
4-nitro-benzoyl chloride

: 99-56-9
4-Nitrophenylene-1,2-diamine

: 70499-97-7
N-(2-amino-5-nitrophenyl)-4-nitrobenzylamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at -40 - 20 ℃;
DOI:10.1021/jo050670t

Reference yield:

: 70499-97-7
N-(2-amino-5-nitrophenyl)-4-nitrobenzylamide

: 866250-97-7
N-(2-amino-5-nitro-phenyl)-4-nitro-thiobenzamide

Guidance literature:: With tetraphosphorus decasulfide; sodium carbonate; In tetrahydrofuran; at 0 - 20 ℃; for 13h;
DOI:10.1021/jo050670t

Reference yield:

: 70499-97-7
N-(2-amino-5-nitrophenyl)-4-nitrobenzylamide

: O-naphth-1-yl 4-nitrothiobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: P₂S₅; Na₂CO₃ / tetrahydrofuran / 13 h / 0 - 20 °C

2: sodium nitrite; aq. acetic acid / 0.75 h / 0 °C

3: 99 percent / Et₃N / CH₂Cl₂ / 20 °C

With tetraphosphorus decasulfide; sodium carbonate; acetic acid; triethylamine; sodium nitrite; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo050670t