Dibenzo(b,e)stannin, 5,10-dihydro-5,5-dimethyl-

Base Information

• Chemical Name: Dibenzo(b,e)stannin, 5,10-dihydro-5,5-dimethyl-
• CAS No.: 23708-66-9
• Molecular Formula: C15H16 Sn
• Molecular Weight: 315.002
• DSSTox Substance ID: DTXSID20178371
• Wikidata: Q83048753
• Mol file: 23708-66-9.mol

Synonyms:Dibenzo(b,e)stannin, 5,10-dihydro-5,5-dimethyl-;23708-66-9;Dibenzo[b,e]stannin,5,10-dihydro-5,5-dimethyl-;DTXSID20178371

Chemical Property of Dibenzo(b,e)stannin, 5,10-dihydro-5,5-dimethyl-

Chemical Property:

• Vapor Pressure: 0.000166mmHg at 25°C
• Boiling Point: 340.7°Cat760mmHg
• Flash Point: 164.1°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 316.027403
• Heavy Atom Count: 16
• Complexity: 234

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Sn]1(C2=CC=CC=C2CC3=CC=CC=C31)C

Technology Process of Dibenzo(b,e)stannin, 5,10-dihydro-5,5-dimethyl-

There total 3 articles about Dibenzo(b,e)stannin, 5,10-dihydro-5,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2,2’-dibromodiphenylmethane (61592-89-0) + dimethyltin dichloride (753-73-1) → 5,5-dimethyl-5,10-dihydrodibenzo[b,e]stannine (23708-66-9)

Guidance literature:

2,2’-dibromodiphenylmethane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1.5h;

dimethyltin dichloride; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1021/acs.orglett.1c01983

Reference yield: 55.1%

dimethyltin dichloride (753-73-1) + CH2(C6H4MgCl)2 → 5,5-dimethyl-5,10-dihydrodibenzo[b,e]stannine (23708-66-9)

Guidance literature:

In tetrahydrofuran; boiling, 4h;;

DOI:10.1016/S0022-328X(00)87735-9

Reference yield:

→ 5,5-dimethyl-5,10-dihydrodibenzo[b,e]stannine (23708-66-9)

Guidance literature:

Digrignard v. o,o'-Dichlordiphenylmethan, Dimethyl-zinndichlorid;

DOI:10.1016/S0022-328X(00)87735-9

upstream raw materials:

dimethyltin dichloride

2,2’-dibromodiphenylmethane

Downstream raw materials:

9-phenyl-9,10-dihydro-9-borataanthracene

dimethyltin dichloride

9-bora-9-chloro-9,10-dihydroanthracene

9-boraanthracene-H₂IMes

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