2-chloro-N,N-di(propan-2-yl)benzamide

Base Information

Chemical Name:2-chloro-N,N-di(propan-2-yl)benzamide
CAS No.:70657-63-5
Molecular Formula:C13H18ClNO
Molecular Weight:239.745
Hs Code.:
DSSTox Substance ID:DTXSID90877263
Nikkaji Number:J419.209E
Wikidata:Q82859021
Mol file:70657-63-5.mol

Synonyms:2-chloro-N,N-di(propan-2-yl)benzamide;70657-63-5;2-Chloro-N,N-diisopropylbenzamide;starbld0007567;2-Chloro-N,N-diisopropylbenzamid;DTXSID90877263;N,N-Diisopropyl-2-chlorobenzamide;STK447596;AKOS003236952;2-Chloro-N,N-bis(1-isopropyl)benzamide;2-chloro-N,N-bis(propan-2-yl)benzamide;2-Chloro-N,N-bis(1-methylethyl)benzamide;Benzamide, 2-chloro-N,N-bis(1-methylethyl)-;Z276695112

Suppliers and Price of 2-chloro-N,N-di(propan-2-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-chloro-N,N-di(propan-2-yl)benzamide

Chemical Property:

Boiling Point:347.6±25.0 °C(Predicted)
PKA:-1.54±0.70(Predicted)
PSA：20.31000
Density:1.072±0.06 g/cm3(Predicted)
LogP:3.59900
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:239.1076919
Heavy Atom Count:16
Complexity:232

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)N(C(C)C)C(=O)C1=CC=CC=C1Cl

Technology Process of 2-chloro-N,N-di(propan-2-yl)benzamide

There total 4 articles about 2-chloro-N,N-di(propan-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 20383-28-2
N,N-diisopropyl benzamide

: 70657-63-5
N,N-diisopropyl 2-chlorobenzamide

Guidance literature:: N,N-diisopropyl benzamide; With (2,2,6,6-tetramethylpiperidido)₂Ag(CN)Li₂; at 0 ℃; for 0.5h;

With N-chlorophthalimide; at 20 ℃; for 1h; Reagent/catalyst; chemoselective reaction;
DOI:10.1039/c9sc06060j

Reference yield: 88.0%

: 609-65-4
o-chlorobenzoyl chloride

: 108-18-9
diisopropylamine

: 70657-63-5
N,N-diisopropyl 2-chlorobenzamide

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1002/anie.201809929

Reference yield: 2.0%

: 20383-28-2
N,N-diisopropyl benzamide

: 5440-69-7
N-isopropylbenzamide

: 70657-63-5
N,N-diisopropyl 2-chlorobenzamide

: 35306-66-2
N,N-diisopropyl 3-chlorobenzamide

: 79606-45-4
N,N-diisopropyl 4-chlorobenzamide

: 65-85-0,8013-63-6
benzoic acid

: 535-80-8
3-chlorobenzoate

Guidance literature:: With chlorine; In sulfolane; water; at 50 ℃; for 9h; Product distribution; different benzoic acid derivatives and chlorination or bromination conditions;
DOI:10.1002/(sici)1099-0690(199808)1998:8<1689::aid-ejoc1689>3.0.co;2-m