3-Methylbenzoyl azide

Base Information

Chemical Name:3-Methylbenzoyl azide
CAS No.:71313-13-8
Molecular Formula:C8H7N3O
Molecular Weight:161.163
Hs Code.:
DSSTox Substance ID:DTXSID90502568
Nikkaji Number:J808.109C
Wikidata:Q82355723

Synonyms:3-Methylbenzoyl azide;71313-13-8;SCHEMBL19398201;DTXSID90502568;AKOS009453572

Suppliers and Price of 3-Methylbenzoyl azide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 3-Methylbenzoyl azide

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:161.058911855
Heavy Atom Count:12
Complexity:220

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)C(=O)N=[N+]=[N-]

Technology Process of 3-Methylbenzoyl azide

There total 6 articles about 3-Methylbenzoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1711-06-4
3-Methylbenzoyl chloride

: 71313-13-8
3-methylbenzoyl azide

Guidance literature:: With trimethylsilylazide; zinc(II) iodide; In dichloromethane; 1.) 0 deg C, 30 min, 2.) room temp., 3 h;
DOI:10.1021/jo00167a051

Reference yield: 92.0%

: 201230-82-2
carbon monoxide

: 625-95-6
3-Iodotoluene

: 71313-13-8
3-methylbenzoyl azide

Guidance literature:: With sodium azide; [Pd₂(dba)5]; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; hexane; water; at 23 ℃; for 2.5h; under 760.051 Torr;
DOI:10.1002/anie.201200078

Reference yield: 92.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 625-95-6
3-Iodotoluene

: 71313-13-8
3-methylbenzoyl azide

Guidance literature:: With sodium azide; C₃₉H₃₂Cl₂OP₂Pd*CH₂Cl₂; In tetrahydrofuran; hexane; water; at 20 ℃; under 760.051 Torr;
DOI:10.1021/om401126m