1-benzyl-3-cyanopyridinium chloride

Base Information

• Chemical Name: 1-benzyl-3-cyanopyridinium chloride
• CAS No.: 14535-08-1
• Molecular Formula: C13H11 N2 . Cl
• Molecular Weight: 230.6928
• Mol file: 14535-08-1.mol

Synonyms:1-Benzyl-3-cyanopyridiniumchloride (7CI); Pyridinium, 1-benzyl-3-cyano-, chloride (8CI); Pyridinium, 3-cyano-1-(phenylmethyl)-,chloride (9CI); N1-Benzyl-3-cyanopyridinium chloride

Chemical Property of 1-benzyl-3-cyanopyridinium chloride

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-benzyl-3-cyanopyridinium chloride

There total 1 articles about 1-benzyl-3-cyanopyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

pyridine-3-carbonitrile (100-54-9,121697-66-3,1232169-17-3,68271-95-4) + benzyl chloride (100-44-7) → 3-cyano-1-benzylpyridinium chloride (14535-08-1)

Guidance literature:

at 60 - 70 ℃; for 24h;

Reference yield: 85.0%

piperidine (110-89-4) + 3-cyano-1-benzylpyridinium chloride (14535-08-1) → 1'-Benzyl-3,4,5,6,1',2'-hexahydro-2H-[1,2']bipyridinyl-5'-carbonitrile (75340-24-8)

Guidance literature:

In neat (no solvent); for 2h; Ambient temperature;

DOI:10.1016/S0040-4020(01)93695-6

Reference yield: 79.0%

3-(5-amino-3-methylpyrazol-1-yl)propionitrile (61255-82-1) + 3-cyano-1-benzylpyridinium chloride (14535-08-1) → 4-[5-amino-1-(2-cyano-ethyl)-3-methyl-1H-pyrazol-4-yl]-1-benzyl-1,4-dihydro-pyridine-3-carbonitrile

Guidance literature:

With triethylamine; In methanol; at 4 ℃; for 24h;

DOI:10.1016/S0040-4039(02)02508-X

upstream raw materials:

pyridine-3-carbonitrile

benzyl chloride

Downstream raw materials:

1'-Benzyl-3,4,5,6,1',2'-hexahydro-2H-[1,2']bipyridinyl-5'-carbonitrile

1-benzyl-1,6-dihydropyridine-3-carbonitrile

1-benzyl-1,4-dihydropyridine-3-carbonitrile

1-benzyl-1,4,5,6-tetrahydropyridine-3-carboxamide

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