Benzenemethanamine, 3,4-dimethoxy-N-(phenylmethylene)-

Base Information

• Chemical Name: Benzenemethanamine, 3,4-dimethoxy-N-(phenylmethylene)-
• CAS No.: 71703-43-0
• Molecular Formula: C16H17NO2
• Molecular Weight: 255.316
• DSSTox Substance ID: DTXSID70471420
• Nikkaji Number: J1.393.330H

Synonyms:71703-43-0;Benzenemethanamine, 3,4-dimethoxy-N-(phenylmethylene)-;DTXSID70471420

Chemical Property of Benzenemethanamine, 3,4-dimethoxy-N-(phenylmethylene)-

Chemical Property:

• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 255.125928785
• Heavy Atom Count: 19
• Complexity: 274

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=C(C=C1)CN=CC2=CC=CC=C2)OC

Technology Process of Benzenemethanamine, 3,4-dimethoxy-N-(phenylmethylene)-

There total 4 articles about Benzenemethanamine, 3,4-dimethoxy-N-(phenylmethylene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

3,4-dimethoxybenzylamine (5763-61-1) + benzyl alcohol (100-51-6,185532-71-2) → N-(3,4-dimethoxybenzyl)benzamide (20781-28-6) + benzylidene-3,4-dimethoxybenzylamine (71703-43-0)

Guidance literature:

With C₂₆H₃₆ClN₂RuS⁽¹⁺⁾*F₆P^(1-); caesium carbonate; In toluene; at 125 ℃; for 36h; Schlenk technique; Inert atmosphere;

DOI:10.1002/ejic.202101033

Reference yield:

benzaldehyde (100-52-7) + 3,4-dimethoxybenzylamine (5763-61-1) → benzylidene-3,4-dimethoxybenzylamine (71703-43-0)

Guidance literature:

With magnesium sulfate; In benzene; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)80532-9

Reference yield:

benzaldehyde (100-52-7) + 3,4-dimethoxybenzylamine (5763-61-1) → (3,4-Dimethoxy-benzyl)-[1-phenyl-meth-(Z)-ylidene]-amine (71703-43-0)

Guidance literature:

DOI:10.1016/S0040-4020(01)88885-2

upstream raw materials:

benzaldehyde

3,4-dimethoxybenzylamine

benzyl alcohol

Downstream raw materials:

C₁₇H₁₈NO₃⁽¹⁺⁾

cis-3-Phenoxyacetylamino-4-phenyl-2-azetidinone

3-phenylacetamido-4-phenylazetidin-2-one

N-[(3S,4R)-1-(3,4-Dimethoxy-benzyl)-2-oxo-4-phenyl-azetidin-3-yl]-2-phenyl-acetamide

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