Ethyl bicyclo[6.1.0]nonane-9-carboxylate

Base Information

Chemical Name:Ethyl bicyclo[6.1.0]nonane-9-carboxylate
CAS No.:72258-12-9
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:
DSSTox Substance ID:DTXSID40509688
Nikkaji Number:J1.688.310G

Synonyms:ethyl bicyclo[6.1.0]nonane-9-carboxylate;72258-12-9;Bicyclo[6.1.0]nonane-9-carboxylic acid, ethyl ester;bicyclo[6.1.0]nonane-9-carboxylic acid ethyl ester;SCHEMBL3983188;DTXSID40509688;AKOS024321838

Suppliers and Price of Ethyl bicyclo[6.1.0]nonane-9-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Ethyl bicyclo[6.1.0]nonane-9-carboxylate

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:196.146329876
Heavy Atom Count:14
Complexity:198

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1C2C1CCCCCC2

Technology Process of Ethyl bicyclo[6.1.0]nonane-9-carboxylate

There total 3 articles about Ethyl bicyclo[6.1.0]nonane-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 623-73-4
diazoacetic acid ethyl ester

: 931-88-4,22770-27-0,3958-30-3,25267-51-0
1,2-cyclooctene

: 72258-12-9,923952-55-0
ethyl bicycle[6.1.0]nonane-9-carboxylate

: 623-91-6
diethyl Fumarate

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; C₃₀H₂₈N₂*Cu⁽¹⁺⁾*F₆P^(1-); In chloroform-d1; at 55 ℃; for 4h; Reagent/catalyst;
DOI:10.1039/c4dt01508h

Reference yield: 49.0%

: 623-73-4
diazoacetic acid ethyl ester

: 931-88-4,22770-27-0,3958-30-3,25267-51-0
1,2-cyclooctene

: 72258-12-9,923952-55-0
ethyl bicycle[6.1.0]nonane-9-carboxylate

: 623-91-6
diethyl Fumarate

: 141-05-9
Diethyl maleate

Guidance literature:: 1,2-cyclooctene; With [3-methyl-1-(4-methylenehex-5-enyl)-1H-imidazolidene][η⁶-(p-cymene)]RuCl₂; at 60 ℃; for 0.25h; Schlenk technique; Inert atmosphere;

diazoacetic acid ethyl ester; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejic.201500054