1-{Diphenyl[2-(pyrrolidin-1-yl)ethyl]silyl}pyrrolidine

Base Information

Chemical Name:1-{Diphenyl[2-(pyrrolidin-1-yl)ethyl]silyl}pyrrolidine
CAS No.:72385-48-9
Molecular Formula:C22H30N2Si
Molecular Weight:350.579
Hs Code.:
DSSTox Substance ID:DTXSID50501779
Wikidata:Q82354372

Synonyms:72385-48-9;1-{Diphenyl[2-(pyrrolidin-1-yl)ethyl]silyl}pyrrolidine;DTXSID50501779

Suppliers and Price of 1-{Diphenyl[2-(pyrrolidin-1-yl)ethyl]silyl}pyrrolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-{Diphenyl[2-(pyrrolidin-1-yl)ethyl]silyl}pyrrolidine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:350.217825500
Heavy Atom Count:25
Complexity:371

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCN(C1)CC[Si](C2=CC=CC=C2)(C3=CC=CC=C3)N4CCCC4

Technology Process of 1-{Diphenyl[2-(pyrrolidin-1-yl)ethyl]silyl}pyrrolidine

There total 2 articles about 1-{Diphenyl[2-(pyrrolidin-1-yl)ethyl]silyl}pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 123-75-1
pyrrolidine

: 18419-53-9
vinyldiphenylchlorosilane

: 72385-48-9
Diphenylpyrrolidino(2-pyrrolidinoethyl)silan

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/ardp.19843170305

Reference yield:

: phenylmagnesium chloride

: 72385-48-9
Diphenylpyrrolidino(2-pyrrolidinoethyl)silan

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / diethyl ether; tetrahydrofuran / 20 deg C, 50 h; reflux, 8 h

2: 68 percent / n-Butyllithium / tetrahydrofuran; hexane

With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1002/ardp.19843170305