4,4'-Bipyridinium, 1-(phenylmethyl)-, bromide

Base Information

• Chemical Name: 4,4'-Bipyridinium, 1-(phenylmethyl)-, bromide
• CAS No.: 72433-69-3
• Molecular Formula: C17H15N2.Br
• Molecular Weight: 327.224

Synonyms:

Chemical Property of 4,4'-Bipyridinium, 1-(phenylmethyl)-, bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4'-Bipyridinium, 1-(phenylmethyl)-, bromide

There total 2 articles about 4,4'-Bipyridinium, 1-(phenylmethyl)-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4,4'-bipyridine (553-26-4) + benzyl bromide (100-39-0) → 1-benzyl-4-(4-pyridyl)pyridinium bromide (72433-69-3)

Guidance literature:

In dichloromethane; at 60 ℃; for 1h; Microwave irradiation;

DOI:10.1016/j.tetlet.2010.08.070

Reference yield:

4,4'-bipyridine (553-26-4) + benzyl bromide (100-39-0) → 1-benzyl-4-(4-pyridyl)pyridinium bromide (72433-69-3) + 1,1’-bis(phenylmethyl)-4,4’bipyridinium bromide (27768-49-6)

Guidance literature:

In acetonitrile; for 24h; Heating;

DOI:10.1080/15421400490478272

Reference yield: 89.0%

1-benzyl-4-(4-pyridyl)pyridinium bromide (72433-69-3) → C18H18N2(2+) (70293-19-5)

Guidance literature:

In acetonitrile; at 130 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1016/j.tetlet.2010.08.070

upstream raw materials:

4,4'-bipyridine

benzyl bromide

Downstream raw materials:

1-benzyl-1'-heptyl-4,4'-bipyridinium bromide

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