Ethyl [2-(3-methylbut-2-en-1-yl)phenyl]carbamate

Base Information

Chemical Name:Ethyl [2-(3-methylbut-2-en-1-yl)phenyl]carbamate
CAS No.:72844-93-0
Molecular Formula:C14H19NO2
Molecular Weight:233.31
Hs Code.:
DSSTox Substance ID:DTXSID70504989
Nikkaji Number:J1.329.973K

Synonyms:72844-93-0;Ethyl [2-(3-methylbut-2-en-1-yl)phenyl]carbamate;DTXSID70504989

Suppliers and Price of Ethyl [2-(3-methylbut-2-en-1-yl)phenyl]carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl [2-(3-methylbut-2-en-1-yl)phenyl]carbamate

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:233.141578849
Heavy Atom Count:17
Complexity:269

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)NC1=CC=CC=C1CC=C(C)C

Technology Process of Ethyl [2-(3-methylbut-2-en-1-yl)phenyl]carbamate

There total 4 articles about Ethyl [2-(3-methylbut-2-en-1-yl)phenyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 27125-61-7
2-(3-methylbut-2-en-1-yl)aniline

: 541-41-3
chloroformic acid ethyl ester

: 72844-93-0
ethyl N-<2-(3-methylbut-2-enyl)phenyl>carbamate

Guidance literature:: DOI:10.1021/jo01299a019

Reference yield:

: 2727-71-1
N-(2-bromophenyl)-2,2,2-trifluoroacetamide

: 72844-93-0
ethyl N-<2-(3-methylbut-2-enyl)phenyl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) CH₃Li, t-butyllithium, 2.) tetrakis / 1.) THF, -78 deg C, 1 min, 2.) THF, - 78 deg C, 5 min

2: 89 percent / KOH / methanol / 1 h / Heating

3: 87 percent / pyridine / CH₂Cl₂ / 0.17 h

With pyridine; potassium hydroxide; tetrakiscopper(I); methyllithium; tert.-butyl lithium; In methanol; dichloromethane;

Reference yield:

: 130074-91-8
2,2,2-trifluoro-N-<2-(3-methylbut-2-enyl)phenyl>acetamide

: 72844-93-0
ethyl N-<2-(3-methylbut-2-enyl)phenyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / KOH / methanol / 1 h / Heating

2: 87 percent / pyridine / CH₂Cl₂ / 0.17 h

With pyridine; potassium hydroxide; In methanol; dichloromethane;