4-[dibutyl(chloro)stannanyl]butan-2-one

Base Information

Chemical Name:4-[dibutyl(chloro)stannanyl]butan-2-one
CAS No.:65301-77-1
Molecular Formula:C₁₂H₂₅ClOSn
Molecular Weight:339.493
Hs Code.:

Synonyms:

Suppliers and Price of 4-[dibutyl(chloro)stannanyl]butan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[dibutyl(chloro)stannanyl]butan-2-one

Chemical Property:

Vapor Pressure:0.000254mmHg at 25°C
Boiling Point:323.9°Cat760mmHg
Flash Point:149.7°C
Density:g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-[dibutyl(chloro)stannanyl]butan-2-one

There total 2 articles about 4-[dibutyl(chloro)stannanyl]butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5827-70-3
(2-cyanoethyl)tributylstannane

: 65301-77-1
chloro(3-oxobutyl)dibutylstannane

Guidance literature:: Multi-step reaction with 2 steps

1: NH₄Cl / water; diethyl ether

2: 2,6-lutidine; Bu₄NClO₄; molecular sieve 4A / dichloromethane; water

With NH₄Cl; 2,6-lutidine; Bu₄NClO₄; molecular sieve 4A; In diethyl ether; dichloromethane; water;
DOI:10.1021/ja970899t

Reference yield:

: 98746-44-2
(3-oxobutyl)tributylstannane

: 7647-14-5
sodium chloride

: 65301-77-1
chloro(3-oxobutyl)dibutylstannane

Guidance literature:: With 2,6-lutidine; Bu₄NClO₄; molecular sieve 4A; In dichloromethane; water; Electrolysis; divided cell, carbon rod anode, Pt cathode, Sn-compd. and lutidine placed in anodic chamber, const. current (5 mA) on stirring (0°C), NaCl aqueous soln. addn., stirring (several min, 0°C), warming (roomtemp.); mixture in anodic chamber collected, NaCl added, stirring (several min, room temp.), volatiles removal (reduced pressure), Et2O addn., stirring,filtration, org. phase sepn., drying (MgSO4), thin-layer chromy. (silic a gel, hexane:ethyl acetate 10:1);
DOI:10.1021/ja970899t