1,2-Benzenediamine, N-[(4-nitrophenyl)methylene]-

Base Information

• Chemical Name: 1,2-Benzenediamine, N-[(4-nitrophenyl)methylene]-
• CAS No.: 730-29-0
• Molecular Formula: C13H11N3O2
• Molecular Weight: 241.249
• DSSTox Substance ID: DTXSID30479987
• Nikkaji Number: J2.870.206J

Synonyms:730-29-0;1,2-Benzenediamine, N-[(4-nitrophenyl)methylene]-;DTXSID30479987;2-(4-nitrobenzylidene-amino)aniline

Chemical Property of 1,2-Benzenediamine, N-[(4-nitrophenyl)methylene]-

Chemical Property:

• XLogP3: 2.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 241.085126602
• Heavy Atom Count: 18
• Complexity: 306

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)N)N=CC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 1,2-Benzenediamine, N-[(4-nitrophenyl)methylene]-

There total 9 articles about 1,2-Benzenediamine, N-[(4-nitrophenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzaldehyde (100-52-7) + 1,2-diamino-benzene (95-54-5) → N-(4-nitrobenzylidene)-benzene-1,2-diamine (730-29-0)

Guidance literature:

With sodium chloride; for 2h; Concentration; Mechanism; Milling;

DOI:10.1002/jhet.1113

Reference yield: 90.0%

4-nitrobenzaldehdye (555-16-8) + 1,2-diamino-benzene (95-54-5) → N-(4-nitrobenzylidene)-benzene-1,2-diamine (730-29-0)

Guidance literature:

2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; for 24h; Ambient temperature;

DOI:10.1016/0040-4020(95)00252-4

Reference yield: 55.0%

1-nitro-2-(4-nitrophenyl)-1-ethoxycarbonylethene (21646-74-2) + 1,2-diamino-benzene (95-54-5) → N-(4-nitrobenzylidene)-benzene-1,2-diamine (730-29-0)

Guidance literature:

In methanol; for 0.666667h;

DOI:10.1134/S1070363212080117

upstream raw materials:

4-nitrobenzaldehdye

1,2-diamino-benzene

N-pyridinium chloride

1-nitro-2-(4-nitrophenyl)-1-ethoxycarbonylethene

Downstream raw materials:

2-(4-nitrophenyl)benzimidazole

N-p-nitrobenzyl-o-phenylenediamine

2-(2'-Hydroxyphenyl)benzimidazole

2-(2,4-dimethoxyphenyl)-1H-benzo[d]imidazole

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