Methanone, [4-[3-[4-(dimethylamino)phenyl]propyl]phenyl]phenyl-

Base Information

Chemical Name:Methanone, [4-[3-[4-(dimethylamino)phenyl]propyl]phenyl]phenyl-
CAS No.:73060-15-8
Molecular Formula:C24H25NO
Molecular Weight:343.46100
Hs Code.:

Synonyms:4-<3-(4-(N,N-dimethylamino)phenyl)propyl>benzophenone;Methanone,[4-[3-[4-(dimethylamino)phenyl]propyl]phenyl]phenyl;

Suppliers and Price of Methanone, [4-[3-[4-(dimethylamino)phenyl]propyl]phenyl]phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, [4-[3-[4-(dimethylamino)phenyl]propyl]phenyl]phenyl-

Chemical Property:

PSA：20.31000
LogP:5.15890

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanone, [4-[3-[4-(dimethylamino)phenyl]propyl]phenyl]phenyl-

There total 6 articles about Methanone, [4-[3-[4-(dimethylamino)phenyl]propyl]phenyl]phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-3-(4-Dimethylamino-phenyl)-1-[4-(2-phenyl-[1,3]dioxolan-2-yl)-phenyl]-propenone

: 73060-15-8
4-<3-(4-(N,N-dimethylamino)phenyl)propyl>benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 70.5 percent / H₂ / 5percent Pd-C / dioxane

2: hydrazine hydrate, NaOH / bis-(2-hydroxy-ethyl) ether / 1.) reflux, 1 h, 2.) 220 deg C, 4 h

3: 2N HCl / 1 h

With hydrogenchloride; sodium hydroxide; hydrogen; hydrazine hydrate; palladium on activated charcoal; In 1,4-dioxane; diethylene glycol;
DOI:10.1021/ja00393a023

Reference yield:

: 76509-32-5
4-cyanobenzophenone ethylene acetal

: 73060-15-8
4-<3-(4-(N,N-dimethylamino)phenyl)propyl>benzophenone

Guidance literature:: Multi-step reaction with 5 steps

1: 2.)NH₄Cl / 1.) ether, benzene, 60 deg C, 5 h, 2.) 80 deg C, 1 h

2: 80 percent / NaOH / ethanol; H₂O / 40 h / Ambient temperature

3: 70.5 percent / H₂ / 5percent Pd-C / dioxane

4: hydrazine hydrate, NaOH / bis-(2-hydroxy-ethyl) ether / 1.) reflux, 1 h, 2.) 220 deg C, 4 h

5: 2N HCl / 1 h

With hydrogenchloride; sodium hydroxide; hydrogen; ammonium chloride; hydrazine hydrate; palladium on activated charcoal; In 1,4-dioxane; ethanol; water; diethylene glycol;
DOI:10.1021/ja00393a023

Reference yield:

: 76509-33-6
4-acetylbenzophenone ethylene acetal

: 73060-15-8
4-<3-(4-(N,N-dimethylamino)phenyl)propyl>benzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / NaOH / ethanol; H₂O / 40 h / Ambient temperature

2: 70.5 percent / H₂ / 5percent Pd-C / dioxane

3: hydrazine hydrate, NaOH / bis-(2-hydroxy-ethyl) ether / 1.) reflux, 1 h, 2.) 220 deg C, 4 h

4: 2N HCl / 1 h

With hydrogenchloride; sodium hydroxide; hydrogen; hydrazine hydrate; palladium on activated charcoal; In 1,4-dioxane; ethanol; water; diethylene glycol;
DOI:10.1021/ja00393a023