AKOS BBS-00005653

Base Information

• Chemical Name: AKOS BBS-00005653
• CAS No.: 7309-86-6
• Molecular Formula: C₁₂H₁₁NS₃
• Molecular Weight: 265.424
• Mol file: 7309-86-6.mol

Synonyms:4,4-dimethyl-4,5-dihydro-2,3-dithiolo[3,4-c]quinoline-1-thione;4,4-dimethyl-4,5-dihydro-[1,2]dithiolo[3,4-c]quinoline-1-thione;4,5-dihydro-4,4-dimethyl-2,3-dithiolo[3,4-c]quinoline-1-thione;4,4-dimethyl-2,3-dithiolo[5,4-c]-quinoline-1-thione;4,4-Dimethyl-1-thiono-4,5-dihydro-1H-1,2-dithiolo[3,4-c]chinolin;4,4-dimethyl[1,2]dithiolo[3,4-c]quinoline-1-thione;

Chemical Property of AKOS BBS-00005653

Chemical Property:

• PSA: 100.60000
• LogP: 5.00470

Purity/Quality:

98%min ^*data from raw suppliers

4,4-Dimethyl-4,5-dihydro-1H-[1,2]dithiolo-[3,4-c]quinoline-1-thione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BBS-00005653

There total 2 articles about AKOS BBS-00005653 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,4-trimethyl-1,2-dihydroquinoline (147-47-7,26780-96-1,389806-19-3) → 4,5-dihydro-4,4-dimethyl-5H-2,3-dithiolo<5,4-c>-quinoline-1-thione (7309-86-6)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide;

DOI:10.1039/j39680001074

Reference yield:

1,2,3,4-tetrahydro-2,2,4-trimethylquinoline (4497-58-9) → 4,5-dihydro-4,4-dimethyl-5H-2,3-dithiolo<5,4-c>-quinoline-1-thione (7309-86-6)

Guidance literature:

With sulfur; In various solvent(s); Heating; or without solvent, 210-220 deg C, 40-60 min;

DOI:10.1007/BF00953730

Reference yield: 72.0%

4,5-dihydro-4,4-dimethyl-5H-2,3-dithiolo<5,4-c>-quinoline-1-thione (7309-86-6) + dimethyl acetylenedicarboxylate (762-42-5) → C24H23NO8S3

Guidance literature:

In benzene; for 15h; Heating;

DOI:10.1007/BF02324643

upstream raw materials:

2,2,4-trimethyl-1,2-dihydroquinoline

1,2,3,4-tetrahydro-2,2,4-trimethylquinoline

Downstream raw materials:

5-acetyl-4,5-dihydro-4,4-dimethyl-2,3-dithiolo<3,4-c>quinoline-1-thione

4,5-dihydro-5-benzoyl-4,4-dimethyl-2,3-dithiolo<3,4-c>quinoline-1-thione

4-(4-carbethoxy-1,3-dithiol-2-ylidene)-2,2-dimethyl-1,2,3,4-tetrahydroquinoline-3-thione

2-(benzooxazol-2-ylsulfanyl)-1-(4,4-dimethyl-1-thioxo-1,4-dihydro-2,3-dithia-5-aza-cyclopenta[a]naphthalen-5-yl)-ethanone

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