2-Iodo-3,4,5-trimethoxybenzaldehyde

Base Information

Chemical Name:2-Iodo-3,4,5-trimethoxybenzaldehyde
CAS No.:73252-53-6
Molecular Formula:C10H11IO4
Molecular Weight:322.099
Hs Code.:
DSSTox Substance ID:DTXSID80461756
Nikkaji Number:J1.714.435I
Wikidata:Q82286166

Synonyms:73252-53-6;2-iodo-3,4,5-trimethoxybenzaldehyde;Benzaldehyde, 2-iodo-3,4,5-trimethoxy-;SCHEMBL5392822;DTXSID80461756

Suppliers and Price of 2-Iodo-3,4,5-trimethoxybenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Iodo-3,4,5-trimethoxybenzaldehyde

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:321.97021
Heavy Atom Count:15
Complexity:212

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C(=C1)C=O)I)OC)OC

Technology Process of 2-Iodo-3,4,5-trimethoxybenzaldehyde

There total 3 articles about 2-Iodo-3,4,5-trimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 73252-53-6
3,4,5-trimethoxy-2-iodobenzaldehyde

Guidance literature:: With N-iodo-succinimide; trifluoroacetic acid; In acetonitrile; for 6h; Reflux;
DOI:10.3390/molecules181215613

Reference yield: 93.0%

: 64490-45-5
2-iodo-3,4,5-trimethoxybenzyl alcohol

: 73252-53-6
3,4,5-trimethoxy-2-iodobenzaldehyde

Guidance literature:: With dipyridinium dichromate; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1039/P19820000521

Reference yield:

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 73252-53-6
3,4,5-trimethoxy-2-iodobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / iodine, silver trifluoroacetate / CH₂Cl₂ / 4 h

2: 93 percent / pyridinium dichromate / CH₂Cl₂ / 12 h / Ambient temperature

With dipyridinium dichromate; iodine; silver trifluoroacetate; In dichloromethane;
DOI:10.1039/P19820000521