N-[(Methanesulfonyl)oxy]-P,P-diphenylphosphinic amide

Base Information

Chemical Name:N-[(Methanesulfonyl)oxy]-P,P-diphenylphosphinic amide
CAS No.:73452-22-9
Molecular Formula:C13H14NO4PS
Molecular Weight:311.298
Hs Code.:
DSSTox Substance ID:DTXSID10501513
Wikidata:Q82353931

Synonyms:73452-22-9;N-[(Methanesulfonyl)oxy]-P,P-diphenylphosphinic amide;DTXSID10501513

Suppliers and Price of N-[(Methanesulfonyl)oxy]-P,P-diphenylphosphinic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(Methanesulfonyl)oxy]-P,P-diphenylphosphinic amide

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:311.03811610
Heavy Atom Count:20
Complexity:426

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CS(=O)(=O)ONP(=O)(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of N-[(Methanesulfonyl)oxy]-P,P-diphenylphosphinic amide

There total 3 articles about N-[(Methanesulfonyl)oxy]-P,P-diphenylphosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 73452-52-5
N-hydroxy-P,P-diphenylphosphinic amide

: 124-63-0
methanesulfonyl chloride

: 73452-22-9
N-(Diphenylphosphinyl)-hydroxylamin-methylsulfonat

Guidance literature:: With pyridine; for 0.133333h;

Reference yield:

: 1499-21-4
Diphenylphosphinic chloride

: 73452-22-9
N-(Diphenylphosphinyl)-hydroxylamin-methylsulfonat

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) trimethylsilylhydroxylamine, triethylamine, 2.) methanol / 1.) dichloromethane, 1.6 h, RT, 2.) 3 h

2: 79 percent / pyridine / 0.13 h

With pyridine; methanol; trimethylsilylhydroxylamine; triethylamine;