Hexanoic acid, 6-[methyl[4-[(4-nitrophenyl)azo]phenyl]amino]-, 2,3-dihydroxypropyl ester

Base Information

• Chemical Name: Hexanoic acid, 6-[methyl[4-[(4-nitrophenyl)azo]phenyl]amino]-, 2,3-dihydroxypropyl ester
• CAS No.: 73640-37-6
• Molecular Formula: C22H28N4O6
• Molecular Weight: 444.488
• Mol file: 73640-37-6.mol

Synonyms:

Chemical Property of Hexanoic acid, 6-[methyl[4-[(4-nitrophenyl)azo]phenyl]amino]-, 2,3-dihydroxypropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Hexanoic acid, 6-[methyl[4-[(4-nitrophenyl)azo]phenyl]amino]-, 2,3-dihydroxypropyl ester

There total 3 articles about Hexanoic acid, 6-[methyl[4-[(4-nitrophenyl)azo]phenyl]amino]-, 2,3-dihydroxypropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-bromohexanoyl chloride (22809-37-6) → 1-glycerol (73640-37-6)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / CHCl₃

3: 1.) conc. HCl, NaNO₂

With pyridine; hydrogenchloride; sodium nitrite; In chloroform;

DOI:10.1021/ja00527a004

Reference yield:

(2,3-O-isopropylidene)propyl 6-bromohexanoate → 1-glycerol (73640-37-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 1.) conc. HCl, NaNO₂

With hydrogenchloride; sodium nitrite;

DOI:10.1021/ja00527a004

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) + (2,3-O-isopropylidene)propyl 6-(N-methylanilino)hexanoate → 1-glycerol (73640-37-6)

Guidance literature:

With hydrogenchloride; sodium nitrite; Multistep reaction;

DOI:10.1021/ja00527a004

upstream raw materials:

4-nitro-aniline

6-bromohexanoyl chloride

Downstream raw materials:

Icosanoic acid 2-hydroxy-3-(6-{methyl-[4-(4-nitro-phenylazo)-phenyl]-amino}-hexanoyloxy)-propyl ester

Hexadecanoic acid 2-hydroxy-3-(6-{methyl-[4-(4-nitro-phenylazo)-phenyl]-amino}-hexanoyloxy)-propyl ester