[(1,3-Dioxolan-2-yl)methyl](diphenyl)phosphane

Base Information

Chemical Name:[(1,3-Dioxolan-2-yl)methyl](diphenyl)phosphane
CAS No.:73785-74-7
Molecular Formula:C16H17O2P
Molecular Weight:272.284
Hs Code.:
DSSTox Substance ID:DTXSID60502479
Wikidata:Q82355562

Synonyms:73785-74-7;[(1,3-Dioxolan-2-yl)methyl](diphenyl)phosphane;SCHEMBL8574434;DTXSID60502479

Suppliers and Price of [(1,3-Dioxolan-2-yl)methyl](diphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(1,3-Dioxolan-2-yl)methyl](diphenyl)phosphane

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:272.09661678
Heavy Atom Count:19
Complexity:236

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC(O1)CP(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of [(1,3-Dioxolan-2-yl)methyl](diphenyl)phosphane

There total 5 articles about [(1,3-Dioxolan-2-yl)methyl](diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2568-30-1
2-chloromethyl-1,3-dioxolane

: 829-85-6
diphenylphosphane

: 73785-74-7
(diphenylphosphino)acetaldehyde ethylene acetal

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; 1.) 1.5 h, -30 deg C 2.) 15 h, -30 - 20 deg C;

Reference yield: 40.0%

: 5694-68-8
2-hydroxymethyl-1,3-dioxolane

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 73785-74-7
(diphenylphosphino)acetaldehyde ethylene acetal

Guidance literature:: With N,N-dimethyl-aniline; In hexane; for 2h; Heating;
DOI:10.1021/ja00299a045

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 73785-74-7
(diphenylphosphino)acetaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / diethyl ether / overnight

2: hydroquinone / acetonitrile / 80 h / 60 - 70 °C / argon-filled sealed ampul

3: H₂O, KCN / 4 h / Heating

With potassium cyanide; water; hydroquinone; In diethyl ether; acetonitrile;