Benzoyl chloride, 3,5-bis(octyloxy)-

Base Information

• Chemical Name: Benzoyl chloride, 3,5-bis(octyloxy)-
• CAS No.: 73868-56-1
• Molecular Formula: C23H37ClO3
• Molecular Weight: 396.998
• Mol file: 73868-56-1.mol

Synonyms:

Chemical Property of Benzoyl chloride, 3,5-bis(octyloxy)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoyl chloride, 3,5-bis(octyloxy)-

There total 4 articles about Benzoyl chloride, 3,5-bis(octyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-carbomethoxy-3,5-dihydroxybenzene (2150-44-9) → 3,5-dioctylbenzoic acid chloride (73868-56-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 96 percent / K₂CO₃; Adogen 464 / acetone / Heating

2: 86 percent / NaOH / methanol / Heating

3: SOCl₂ / 2 h / Heating

With sodium hydroxide; thionyl chloride; adogen 464; potassium carbonate; In methanol; acetone;

DOI:10.1039/b615545f

Reference yield:

methyl 3,5-bis(octyloxy)benzoate (87963-84-6) → 3,5-dioctylbenzoic acid chloride (73868-56-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / NaOH / methanol / Heating

2: SOCl₂ / 2 h / Heating

With sodium hydroxide; thionyl chloride; In methanol;

DOI:10.1039/b615545f

Reference yield:

1-bromo-octane (111-83-1) → 3,5-dioctylbenzoic acid chloride (73868-56-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃ / acetonitrile / 100 °C

2: 98 percent / KOH / ethanol / 4 h / Heating

3: 100 percent / SOCl₂ / Heating

With potassium hydroxide; thionyl chloride; potassium carbonate; In ethanol; acetonitrile;

DOI:10.1055/s-2004-831241

upstream raw materials:

1-carbomethoxy-3,5-dihydroxybenzene

3,5-Dihydroxybenzoic acid

methyl 3,5-bis(octyloxy)benzoate

1-bromo-octane

Downstream raw materials:

ethyl 3,5-bis(3,5-dioctyloxybenzoylamino)-4-methyl benzoate

1-bromo-3,5-bis(octyloxy)phenyl

3,5-dioctyloxybenzeneboronic acid ethylene glycol ester

3,5-bis-(3,5-bis-octyloxy-benzoylamino)-4-methyl-benzoic acid 9-methyl-[1,10]phenanthrolin-2-ylmethyl ester

Refernces

• 1、 Lian, Wenhui,Sun, Yuanyuan,Wang, Binbin,Shan, Ning,Shi, Tongshun. "Synthesis and properties of 5,10,15,20-tetrakis[4-(3,5-dioctyloxybenzamido) phenyl]porphyrin and its metal complexes". . p. 335 - 348. Retrieved 2012/05/20.
• 2、 Pickaert, Guillaume,Ziessel, Raymond. "Synthesis of oligopyridinic scaffolds from amido substituted phenyl rings for extended hydrogen bonding". . p. 2716 - 2726. Retrieved 2007/10/03.