Technology Process of 3,5-dioctyloxybenzeneboronic acid ethylene glycol ester
There total 10 articles about 3,5-dioctyloxybenzeneboronic acid ethylene glycol ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aq. HCl / tetrahydrofuran; hexane
2: benzene / Heating
With
hydrogenchloride;
In
tetrahydrofuran; hexane; benzene;
DOI:10.1039/b615545f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: tetrahydrofuran; hexane / -78 - 20 °C
2.1: aq. HCl / tetrahydrofuran; hexane
3.1: benzene / Heating
With
hydrogenchloride; n-butyllithium;
In
tetrahydrofuran; hexane; benzene;
DOI:10.1039/b615545f
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 96 percent / K2CO3; Adogen 464 / acetone / Heating
2.1: 86 percent / NaOH / methanol / Heating
3.1: SOCl2 / 2 h / Heating
4.1: 0.70 g / CBrCl3; 2-mercaptopyridine N-oxide sodium salt; AIBN / 1 h / Heating
5.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C
5.2: tetrahydrofuran; hexane / -78 - 20 °C
6.1: aq. HCl / tetrahydrofuran; hexane
7.1: benzene / Heating
With
hydrogenchloride; sodium hydroxide; n-butyllithium; thionyl chloride; adogen 464; 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; potassium carbonate;
In
tetrahydrofuran; methanol; hexane; acetone; benzene;
4.1: Barton decarboxylation;
DOI:10.1039/b615545f
