2-[(2-Phenylethyl)sulfanyl]pyrimidine

Base Information

Chemical Name:2-[(2-Phenylethyl)sulfanyl]pyrimidine
CAS No.:73869-75-7
Molecular Formula:C12H12N2S
Molecular Weight:216.307
Hs Code.:
DSSTox Substance ID:DTXSID60572612
Nikkaji Number:J1.141.255F
Wikidata:Q82461021

Synonyms:73869-75-7;2-[(2-Phenylethyl)sulfanyl]pyrimidine;DTXSID60572612

Suppliers and Price of 2-[(2-Phenylethyl)sulfanyl]pyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(2-Phenylethyl)sulfanyl]pyrimidine

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:216.07211956
Heavy Atom Count:15
Complexity:163

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CCSC2=NC=CC=N2

Technology Process of 2-[(2-Phenylethyl)sulfanyl]pyrimidine

There total 2 articles about 2-[(2-Phenylethyl)sulfanyl]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 622-24-2
2-phenylethyl chloride

: 131242-36-9
2-sulfanylpyrimidine

: 73869-75-7
2-(phenylethylthio)-pyrimidine

Guidance literature:: 2-sulfanylpyrimidine; With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 1h;

2-phenylethyl chloride; In N,N-dimethyl-formamide; at 60 ℃; for 12h;
DOI:10.1021/jacs.1c05479

Reference yield: 59.0%

: 1722-12-9,1195939-87-7
2-chloropyrimidine

: 4410-99-5
2-mercaptophenylethane

: 73869-75-7
2-(phenylethylthio)-pyrimidine

Guidance literature:: With potassium tri-sec-butyl-borohydride; In tetrahydrofuran; 1,2-dimethoxyethane; at 20 ℃;
DOI:10.1016/S0040-4039(99)01038-2

Reference yield:

: 73869-75-7
2-(phenylethylthio)-pyrimidine

: 2-(styrylthio)pyrimidine

: styryl 2-pyrimidyl sulfide

Guidance literature:: With 2-chloroanthracene-9,10-dione; cobalt(II) diacetate tetrahydrate; butane-2,3-dione dioxime; In 1,2-dichloro-ethane; at 20 - 30 ℃; for 36h; Overall yield = 71 percent; Overall yield = 15.2 mg; Irradiation; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.1c05479