9H-Carbazol-1-ol, 7-methyl-

Base Information

• Chemical Name: 9H-Carbazol-1-ol, 7-methyl-
• CAS No.: 73910-77-7
• Molecular Formula: C13H11NO
• Molecular Weight: 197.236
• DSSTox Substance ID: DTXSID80455791
• Nikkaji Number: J1.159.961C
• Wikidata: Q82277929

Synonyms:9H-Carbazol-1-ol, 7-methyl-;73910-77-7;7-methyl-9H-carbazol-1-ol;1-hydroxy-7-methylcarbazole;7-Methyl-9H-carbazole-1-ol;SCHEMBL20434645;DTXSID80455791

Chemical Property of 9H-Carbazol-1-ol, 7-methyl-

Chemical Property:

• Boiling Point: 439.0±25.0 °C(Predicted)
• PSA: 36.02000
• Density: 1.308±0.06 g/cm3(Predicted)
• LogP: 3.33510
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 197.084063974
• Heavy Atom Count: 15
• Complexity: 243

Purity/Quality:

7-methyl-9H-Carbazol-1-ol 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC2=C(C=C1)C3=C(N2)C(=CC=C3)O

Technology Process of 9H-Carbazol-1-ol, 7-methyl-

There total 3 articles about 9H-Carbazol-1-ol, 7-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.2%

1-oxo-7-methyl-1,2,3,4-tetrahydrocarbazole → 2-methyl-9H-carbazole (3652-91-3) + 1-hydroxy-7-methylcarbazole (73910-77-7)

Guidance literature:

With palladium on activated charcoal; In diphenylether; for 1.5h; Heating;

Reference yield:

7-methyl-1-oxo-1,2,3,4-tetrahydrocarbazole (73910-75-5) → 1-hydroxy-7-methylcarbazole (73910-77-7)

Guidance literature:

With palladium on activated charcoal; In diphenylether;

DOI:10.3987/com-99-8587

Reference yield:

C16H15NO4 (1093413-52-5) → 1-hydroxy-7-methylcarbazole (73910-77-7) + 7-methyl-1-oxo-1,2,3,4-tetrahydrocarbazole (73910-75-5)

Guidance literature:

With air; acetic acid; urea;

DOI:10.3184/030823407X266324

upstream raw materials:

7-methyl-1-oxo-1,2,3,4-tetrahydrocarbazole

C₁₆H₁₅NO₄

Downstream raw materials:

1-(1-hydroxy-7-methyl-9H-carbazol-2-yl)-3-phenyl-propenone

9-methyl-2-phenyl-2,3-dihydro-11H-1-oxa-11-aza-benzo[a]fluoren-4-one

8-methyl-3-phenyl-10H-furo[2,3-a]carbazole

2-(7-methyl-9H-carbazol-1-yloxy)-1-phenylethanone

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