1H-Carbazol-1-one, 2,3,4,9-tetrahydro-7-methyl-

Base Information

Chemical Name:1H-Carbazol-1-one, 2,3,4,9-tetrahydro-7-methyl-
CAS No.:73910-75-5
Molecular Formula:C13H13NO
Molecular Weight:199.252
Hs Code.:
DSSTox Substance ID:DTXSID70464357
Wikidata:Q82289644

Synonyms:73910-75-5;1H-Carbazol-1-one, 2,3,4,9-tetrahydro-7-methyl-;7-methyl-2,3,4,9-tetrahydrocarbazol-1-one;DTXSID70464357

Suppliers and Price of 1H-Carbazol-1-one, 2,3,4,9-tetrahydro-7-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
2,3,4,9-tetrahydro-7-methyl-1H-Carbazol-1-one 97.00%
25G
$ 13300.00

AccelPharmtech
2,3,4,9-tetrahydro-7-methyl-1H-Carbazol-1-one 97.00%
5G
$ 5360.00

AccelPharmtech
2,3,4,9-tetrahydro-7-methyl-1H-Carbazol-1-one 97.00%
1G
$ 3120.00

Total 0 raw suppliers

Chemical Property of 1H-Carbazol-1-one, 2,3,4,9-tetrahydro-7-methyl-

Chemical Property:

Melting Point:160-165 °C
Boiling Point:389.1±11.0 °C(Predicted)
PSA：32.86000
Density:1.233±0.06 g/cm3(Predicted)
LogP:2.99530
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:199.099714038
Heavy Atom Count:15
Complexity:276

Purity/Quality:: 2,3,4,9-tetrahydro-7-methyl-1H-Carbazol-1-one 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)C3=C(N2)C(=O)CCC3

Technology Process of 1H-Carbazol-1-one, 2,3,4,9-tetrahydro-7-methyl-

There total 8 articles about 1H-Carbazol-1-one, 2,3,4,9-tetrahydro-7-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093413-52-5
C₁₆H₁₅NO₄

: 73910-77-7
1-hydroxy-7-methylcarbazole

: 73910-75-5
7-methyl-1-oxo-1,2,3,4-tetrahydrocarbazole

Guidance literature:: With air; acetic acid; urea;
DOI:10.3184/030823407X266324

Reference yield:

: C₁₃H₁₃N₃O₂

: 536-89-0
m-tolylhydrazine

: 82463-55-6
5-methyl-2,3,4,9-tetrahydro-carbazol-1-one

: 73910-75-5
7-methyl-1-oxo-1,2,3,4-tetrahydrocarbazole

Guidance literature:: With oxygen; acetic acid; In acetonitrile; at 80 ℃; Overall yield = 0.053 g; regioselective reaction; Green chemistry;
DOI:10.1039/d0gc01514h

Reference yield:

: 89490-05-1,21190-87-4
cyclohex-1-enylboronic acid

: 82463-55-6
5-methyl-2,3,4,9-tetrahydro-carbazol-1-one

: 73910-75-5
7-methyl-1-oxo-1,2,3,4-tetrahydrocarbazole

Guidance literature:: Multi-step reaction with 2 steps

1: copper diacetate; pyridine; sodium sulfate / acetonitrile / 24 h / 20 °C / Green chemistry

2: acetic acid; oxygen / acetonitrile / 80 °C / Green chemistry

With pyridine; oxygen; copper diacetate; acetic acid; sodium sulfate; In acetonitrile;
DOI:10.1039/d0gc01514h