Technology Process of 3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one
There total 3 articles about 3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) sodium / 1.) ethanol, 30 min; 2.) DMF, 150 deg C, 10 h
2: 70 percent / fuming nitric acid (d=1.52), sulfuric acid (d=1.84) / ice cooling
With
sulfuric acid; nitric acid; sodium;
DOI:10.1246/bcsj.57.1961
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) sodium / 1.) ethanol, 30 min; 2.) DMF, 150 deg C, 10 h
2: 70 percent / fuming nitric acid (d=1.52), sulfuric acid (d=1.84) / ice cooling
With
sulfuric acid; nitric acid; sodium;
DOI:10.1246/bcsj.57.1961