3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one

Base Information

Chemical Name:3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one
CAS No.:74197-40-3
Molecular Formula:C11H6N4O7
Molecular Weight:306.191
Hs Code.:
DSSTox Substance ID:DTXSID10505834
Nikkaji Number:J433.753K

Synonyms:74197-40-3;3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one;SCHEMBL11383176;DTXSID10505834

Suppliers and Price of 3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one

Chemical Property:

PSA：159.46000
LogP:3.13170
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:1
Exact Mass:306.02364854
Heavy Atom Count:22
Complexity:553

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1N2C=C(C(=O)C(=C2)[N+](=O)[O-])[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one

There total 3 articles about 3,5-Dinitro-1-(4-nitrophenyl)pyridin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 79228-85-6
1-(4-nitrophenyl)-4-pyridone

: 74197-40-3
3,5-dinitro-1-(p-nitrophenyl)-4-pyridone

Guidance literature:: With sulfuric acid; nitric acid; ice cooling;
DOI:10.1246/bcsj.57.1961

Reference yield:

: 100-00-5
4-chlorobenzonitrile

: 74197-40-3
3,5-dinitro-1-(p-nitrophenyl)-4-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium / 1.) ethanol, 30 min; 2.) DMF, 150 deg C, 10 h

2: 70 percent / fuming nitric acid (d=1.52), sulfuric acid (d=1.84) / ice cooling

With sulfuric acid; nitric acid; sodium;
DOI:10.1246/bcsj.57.1961

Reference yield:

: 626-64-2,157061-69-3
pyridin-4-ol

: 74197-40-3
3,5-dinitro-1-(p-nitrophenyl)-4-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium / 1.) ethanol, 30 min; 2.) DMF, 150 deg C, 10 h

2: 70 percent / fuming nitric acid (d=1.52), sulfuric acid (d=1.84) / ice cooling

With sulfuric acid; nitric acid; sodium;
DOI:10.1246/bcsj.57.1961