2,4-Dinitrobenzaldoxime

Base Information

• Chemical Name: 2,4-Dinitrobenzaldoxime
• CAS No.: 3236-33-7
• Molecular Formula: C7H5N3O5
• Molecular Weight: 211.134
• Hs Code.: 2928000090
• NSC Number: 49163,40895
• DSSTox Substance ID: DTXSID50430055
• Mol file: 3236-33-7.mol

Synonyms:2,4-Dinitrobenzaldoxime;3236-33-7;2,4-dinitrobenzaldehyde oxime;(NE)-N-[(2,4-dinitrophenyl)methylidene]hydroxylamine;NSC40895;(e)-2,4-dinitrobenzaldoxime;2,4-Dinitrobenzaldehyde, oxime;DTXSID50430055;NSC49163;(1E)-2,4-dinitrobenzaldehyde oxime;NSC-40895;NSC-49163;AKOS037655311;PS-10455;N-[(E)-(2,4-Dinitrophenyl)methylidene]hydroxylamine

Chemical Property of 2,4-Dinitrobenzaldoxime

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 376.8°Cat760mmHg
• Flash Point: 181.7°C
• PSA: 124.23000
• Density: 1.62g/cm³
• LogP: 2.35750
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 211.02292027
• Heavy Atom Count: 15
• Complexity: 281

Purity/Quality:

99% ^*data from raw suppliers

2,4-Dinitrobenzaldoxime 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1[N+](=O)[O-])[N+](=O)[O-])C=NO
• Isomeric SMILES: C1=CC(=C(C=C1[N+](=O)[O-])[N+](=O)[O-])/C=N/O

Technology Process of 2,4-Dinitrobenzaldoxime

There total 3 articles about 2,4-Dinitrobenzaldoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dinitrobenzaldehyde (528-75-6) → 2,4-dinitro-benzaldehyde-oxime (3236-33-7)

Guidance literature:

With ethanol; hydroxylamine hydrochloride; sodium carbonate;

Reference yield:

2,4-dinitrotoluene (121-14-2) → 2,4-dinitro-benzaldehyde-oxime (3236-33-7)

Guidance literature:

Multi-step reaction with 2 steps

1: p-nitroso-dialkyl-aniline; alcohol; natrium carbonate / Spaltung mit verd. Salpetersaeure

2: alcohol; natrium carbonate; hydroxylamine hydrochloride

With ethanol; p-nitroso-dialkyl-aniline; hydroxylamine hydrochloride; sodium carbonate;

Reference yield:

→ 2,4-dinitro-benzaldehyde-oxime (3236-33-7)

Guidance literature:

2,4-Dinitrobenzaldehyd, NH2OH*HCl;

upstream raw materials:

2,4-dinitrobenzaldehyde

2,4-dinitrotoluene

Downstream raw materials:

2-hydroxy-4-nitro-benzonitrile

2,4-dinitrobenzonitrile

2,4-dinitrophenyldinitromethane

4-amino-2-nitro-benzaldehyde-oxime