3-(4-Chlorophenyl)-4-oxo-2H-1,4lambda~5~-benzoxazine

Base Information

Chemical Name:3-(4-Chlorophenyl)-4-oxo-2H-1,4lambda~5~-benzoxazine
CAS No.:74413-06-2
Molecular Formula:C14H10ClNO2
Molecular Weight:259.692
Hs Code.:
DSSTox Substance ID:DTXSID20501160
Nikkaji Number:J2.536.394I
Wikidata:Q82353341

Synonyms:74413-06-2;3-(4-Chlorophenyl)-4-oxo-2H-1,4lambda~5~-benzoxazine;DTXSID20501160

Suppliers and Price of 3-(4-Chlorophenyl)-4-oxo-2H-1,4lambda~5~-benzoxazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-Chlorophenyl)-4-oxo-2H-1,4lambda~5~-benzoxazine

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:259.0400063
Heavy Atom Count:18
Complexity:337

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(=[N+](C2=CC=CC=C2O1)[O-])C3=CC=C(C=C3)Cl

Technology Process of 3-(4-Chlorophenyl)-4-oxo-2H-1,4lambda~5~-benzoxazine

There total 1 articles about 3-(4-Chlorophenyl)-4-oxo-2H-1,4lambda~5~-benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74413-06-2
3-(4-chloro-phenyl)-2H-benzo[1,4]oxazine 4-oxide

Guidance literature:: 2-nitrophenoxy-acetophenon 2c, Zn/NH4Cl ;
DOI:10.1016/0040-4020(79)88007-2

Reference yield: 85.0%

: 74413-06-2
3-(4-chloro-phenyl)-2H-benzo[1,4]oxazine 4-oxide

: 100-58-3
phenylmagnesium bromide

: 3-p-chlorophenyl-3-phenyl-2H-benzo[1,4]oxazin-4-oxyl

Guidance literature:: 3-(4-chloro-phenyl)-2H-benzo[1,4]oxazine 4-oxide; phenylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With lead dioxide; for 1h;
DOI:10.1021/jo2014559

Reference yield: 80.0%

: 1589-82-8
phenylmagnesium bromide

: 74413-06-2
3-(4-chloro-phenyl)-2H-benzo[1,4]oxazine 4-oxide

: 3-benzyl-3-p-chlorophenyl-2H-benzo[1,4]oxazin-4-oxyl

Guidance literature:: phenylmagnesium bromide; 3-(4-chloro-phenyl)-2H-benzo[1,4]oxazine 4-oxide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With lead dioxide; for 1h; Temperature; Kinetics; Activation energy;
DOI:10.1021/jo2014559