N-[2-(2-Methylprop-2-en-1-yl)phenyl]prop-2-enamide

Base Information

Chemical Name:N-[2-(2-Methylprop-2-en-1-yl)phenyl]prop-2-enamide
CAS No.:74590-91-3
Molecular Formula:C13H15NO
Molecular Weight:201.268
Hs Code.:
DSSTox Substance ID:DTXSID80504950
Nikkaji Number:J2.299.075F
Wikidata:Q82359740

Synonyms:74590-91-3;N-[2-(2-Methylprop-2-en-1-yl)phenyl]prop-2-enamide;DTXSID80504950

Suppliers and Price of N-[2-(2-Methylprop-2-en-1-yl)phenyl]prop-2-enamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(2-Methylprop-2-en-1-yl)phenyl]prop-2-enamide

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:201.115364102
Heavy Atom Count:15
Complexity:257

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C)CC1=CC=CC=C1NC(=O)C=C

Technology Process of N-[2-(2-Methylprop-2-en-1-yl)phenyl]prop-2-enamide

There total 4 articles about N-[2-(2-Methylprop-2-en-1-yl)phenyl]prop-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 59816-87-4
2-(2-methylprop-2-en-1-yl)aniline

: 814-68-6,25189-84-8
acryloyl chloride

: 74590-91-3
N-acryloyl-2-(2-methyl-2-propenyl)aniline

Guidance literature:: With pyridine; In diethyl ether; 1.) 0 deg C, 2.) room temperature, 4 h;
DOI:10.1021/ja00530a044

Reference yield:

: 882788-93-4
N,N-diallyl-2-(2-methylprop-2-en-1-yl)aniline

: 74590-91-3
N-acryloyl-2-(2-methyl-2-propenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethylbarbituruc acid; Pd(PPh₃)4 / CH₂Cl₂ / 16 h / 35 °C

2: pyridine / CH₂Cl₂ / 12 h / 0 - 20 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; In dichloromethane;
DOI:10.1021/ja060291x

Reference yield:

: 615-43-0
2-iodophenylamine

: 74590-91-3
N-acryloyl-2-(2-methyl-2-propenyl)aniline

Guidance literature:: Multi-step reaction with 4 steps

1.1: K₂CO₃ / acetonitrile / Heating

2.1: i-PrMgCl*LiCl / tetrahydrofuran / 0.5 h / -10 °C

2.2: 100 percent / CuCN*LiCl / tetrahydrofuran / 12 h / -10 - 20 °C

3.1: N,N-dimethylbarbituruc acid; Pd(PPh₃)4 / CH₂Cl₂ / 16 h / 35 °C

4.1: pyridine / CH₂Cl₂ / 12 h / 0 - 20 °C

With pyridine; TurboGrignard; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; potassium carbonate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ja060291x