alpha-(Methylnitrosoamino)benzeneacetic acid

Base Information

Chemical Name:alpha-(Methylnitrosoamino)benzeneacetic acid
CAS No.:74641-61-5
Molecular Formula:C9H10N2O3
Molecular Weight:194.19
Hs Code.:
DSSTox Substance ID:DTXSID701277247

Synonyms:alpha-(Methylnitrosoamino)benzeneacetic acid;DTXSID701277247;74641-61-5

Suppliers and Price of alpha-(Methylnitrosoamino)benzeneacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of alpha-(Methylnitrosoamino)benzeneacetic acid

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:194.06914219
Heavy Atom Count:14
Complexity:214

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C(C1=CC=CC=C1)C(=O)O)N=O

Technology Process of alpha-(Methylnitrosoamino)benzeneacetic acid

There total 4 articles about alpha-(Methylnitrosoamino)benzeneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.2%

: 28544-42-5
2-(methylamino)-2-phenylethanoic acid hydrochloride

: 74641-61-5
N-Methyl-N-nitroso-2-phenylglycin

Guidance literature:: With dinitrogen tetraoxide; In water; for 10h;
DOI:10.1002/hlca.19800630312

Reference yield:

: 41470-36-4
α-(Methylamino)-phenylacetonitril

: 74641-61-5
N-Methyl-N-nitroso-2-phenylglycin

Guidance literature:: Multi-step reaction with 3 steps

1: 61.9 percent / formic acid, HCl-gas / 5 h / 45 °C

2: 99.1 percent / HCl / 1 h / Heating

3: 75.2 percent / N₂O₄ / H₂O / 10 h

With hydrogenchloride; formic acid; dinitrogen tetraoxide; In water;
DOI:10.1002/hlca.19800630312

Reference yield:

: 532-28-5,613-88-7
(RS)-mandelonitrile

: 74641-61-5
N-Methyl-N-nitroso-2-phenylglycin

Guidance literature:: Multi-step reaction with 4 steps

1: 99.2 percent / methanol / 2 h / 40 - 50 °C

2: 61.9 percent / formic acid, HCl-gas / 5 h / 45 °C

3: 99.1 percent / HCl / 1 h / Heating

4: 75.2 percent / N₂O₄ / H₂O / 10 h

With hydrogenchloride; formic acid; dinitrogen tetraoxide; In methanol; water;
DOI:10.1002/hlca.19800630312