1-(3,4-Dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxyisoquinolinium chloride

Base Information

Chemical Name:1-(3,4-Dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxyisoquinolinium chloride
CAS No.:5884-22-0
Molecular Formula:C20H23 N O4 . Cl H
Molecular Weight:377.868
Hs Code.:2933499090
European Community (EC) Number:227-560-0
DSSTox Substance ID:DTXSID30974346
NSC Number:118078
Mol file:5884-22-0.mol

Synonyms:1-(3,4-dimethoxybenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline hydrochloride;3,4-dihydropapaverine;3,4-dihydropapaverine, monohydrobromide;3,4-dihydropapaverine, monohydrochloride

Suppliers and Price of 1-(3,4-Dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxyisoquinolinium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-[(3,4-DIMETHOXYPHENYL)METHYL]-6,7-DIMETHOXY-3,4-DIHYDROISOQUINOLINE HYDROCHLORIDE 95.00%
1G
$ 645.95

American Custom Chemicals Corporation
1-[(3,4-DIMETHOXYPHENYL)METHYL]-6,7-DIMETHOXY-3,4-DIHYDROISOQUINOLINE HYDROCHLORIDE 95.00%
5G
$ 920.78

American Custom Chemicals Corporation
1-[(3,4-DIMETHOXYPHENYL)METHYL]-6,7-DIMETHOXY-3,4-DIHYDROISOQUINOLINE HYDROCHLORIDE 95.00%
10G
$ 1321.97

Total 38 raw suppliers

Chemical Property of 1-(3,4-Dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxyisoquinolinium chloride

Chemical Property:

Vapor Pressure:5.28E-09mmHg at 25°C
Melting Point:202ºC
Boiling Point:482.6°Cat760mmHg
Flash Point:196.9°C
PSA：49.28000
Density:g/cm³
LogP:3.54650
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:377.1393859
Heavy Atom Count:26
Complexity:455

Purity/Quality:

99% ^*data from raw suppliers

1-[(3,4-DIMETHOXYPHENYL)METHYL]-6,7-DIMETHOXY-3,4-DIHYDROISOQUINOLINE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CC2=NCCC3=CC(=C(C=C32)OC)OC)OC.Cl

Technology Process of 1-(3,4-Dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxyisoquinolinium chloride

There total 5 articles about 1-(3,4-Dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxyisoquinolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 139-76-4
N-(3,4-dimethoxyphenethyl)-2-(3,4-dimethoxyphenyl)acetamide

: 5884-22-0
1-(3,4-dimethoxybenzyl)-6,7-dimethoxy-3.4-dihydroisoquinoline hydrochloride

Guidance literature:: N-(3,4-dimethoxyphenethyl)-2-(3,4-dimethoxyphenyl)acetamide; With trichlorophosphate; In toluene; at 20 ℃; for 1h; Reflux; Inert atmosphere;

With hydrogenchloride;
DOI:10.1021/acs.joc.9b01604

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 5884-22-0
1-(3,4-dimethoxybenzyl)-6,7-dimethoxy-3.4-dihydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Reflux

2: trichlorophosphate / acetonitrile / 17 h / 20 - 80 °C

With trichlorophosphate; In toluene; acetonitrile;

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 5884-22-0
1-(3,4-dimethoxybenzyl)-6,7-dimethoxy-3.4-dihydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Reflux

2: trichlorophosphate / acetonitrile / 17 h / 20 - 80 °C

With trichlorophosphate; In toluene; acetonitrile;