3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(2-chloro-4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)

Base Information

Chemical Name:3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(2-chloro-4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)
CAS No.:74712-86-0
Molecular Formula:C₆H₁₅N*C₃₈H₃₇ClN₃O₁₁P
Molecular Weight:879.344
Hs Code.:

3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-,
mono[2-(2-chloro-4-nitrophenyl)ethyl] ester, compd. with
N,N-diethylethanamine (1:1)

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Chemical Property of 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(2-chloro-4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)

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Technology Process of 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(2-chloro-4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)

There total 3 articles about 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(2-chloro-4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 74706-79-9
Phosphoric acid 2-(2-chloro-4-nitro-phenyl)-ethyl ester 2,5-dichloro-phenyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

: 121-44-8
triethylamine

: 74712-86-0
Phosphoric acid 2-(2-chloro-4-nitro-phenyl)-ethyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester; compound with triethyl-amine

Guidance literature:: With 4-nitrobenzaldehyde oxime;
DOI:10.1016/S0040-4039(00)71364-5

Reference yield:

: 69395-15-9
2-(2-chloro-4-nitro-phenyl)-ethanol

: 74712-86-0
Phosphoric acid 2-(2-chloro-4-nitro-phenyl)-ethyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 1,2,4-triazole

2: 90 percent / p-nitrobenzaldoxime

With 1,2,4-Triazole; 4-nitrobenzaldehyde oxime;
DOI:10.1016/S0040-4039(00)71364-5

Reference yield:

: 42926-80-7
5'-O-(4-monomethoxytrityl)-2'-deoxythymidine

: 74712-86-0
Phosphoric acid 2-(2-chloro-4-nitro-phenyl)-ethyl ester (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 1,2,4-triazole

2: 90 percent / p-nitrobenzaldoxime

With 1,2,4-Triazole; 4-nitrobenzaldehyde oxime;
DOI:10.1016/S0040-4039(00)71364-5