N,N'-Anthraquinone-1,5-diyldi(oxamic acid)

Base Information

• Chemical Name: N,N'-Anthraquinone-1,5-diyldi(oxamic acid)
• CAS No.: 82-19-9
• Molecular Formula: C18H10N2O8
• Molecular Weight: 382.286
• European Community (EC) Number: 201-402-0
• DSSTox Substance ID: DTXSID70231506
• Nikkaji Number: J192.598I
• Wikidata: Q83112447
• Mol file: 82-19-9.mol

Synonyms:N,N'-Anthraquinone-1,5-diyldi(oxamic acid);82-19-9;EINECS 201-402-0;Acetic acid, 2,2'-((9,10-dihydro-9,10-dioxo-1,5-anthracenediyl)diimino)bis(2-oxo-;Acetic acid, 2,2'-[(9,10-dihydro-9,10-dioxo-1,5-anthracenediyl)diimino]bis[2-oxo-;DTXSID70231506;N,N'-anthraquinon-1,5-diyldioxamsyre;Oxamic acid, N,N'-1,5-anthraquinonylenedi-;2,2'-[(9,10-Dihydro-9,10-dioxo-1,5-anthracenediyl)diimino]bis(2-oxoacetic acid)

Chemical Property of N,N'-Anthraquinone-1,5-diyldi(oxamic acid)

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.782g/cm³
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 4
• Exact Mass: 382.04371528
• Heavy Atom Count: 28
• Complexity: 686

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC2=C(C(=C1)NC(=O)C(=O)O)C(=O)C3=C(C2=O)C(=CC=C3)NC(=O)C(=O)O

Technology Process of N,N'-Anthraquinone-1,5-diyldi(oxamic acid)

There total 2 articles about N,N'-Anthraquinone-1,5-diyldi(oxamic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-diaminoanthraquinone (129-44-2) + oxalic acid (144-62-7,97993-78-7) → N,N'-(9,10-dioxo-9,10-dihydro-anthracene-1,5-diyl)-bis-oxalamic acid (82-19-9)

Guidance literature:

at 100 - 160 ℃;

Reference yield:

1.5-dinitroanthraquinone (82-35-9) → N,N'-(9,10-dioxo-9,10-dihydro-anthracene-1,5-diyl)-bis-oxalamic acid (82-19-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium sulfide

2: 100 - 160 °C

With sodium sulfide;

Reference yield:

N,N'-(9,10-dioxo-9,10-dihydro-anthracene-1,5-diyl)-bis-oxalamic acid (82-19-9) → 1,4,5,8-tetraaminoanthraquinone (2475-45-8)

Guidance literature:

Multi-step reaction with 3 steps

1: concentrated sulfuric acid; nitric acid

2: natrium carbonate

3: sodium sulfide

With sodium sulfide; sulfuric acid; nitric acid; sodium carbonate;

upstream raw materials:

1,5-diaminoanthraquinone

oxalic acid

1.5-dinitroanthraquinone

Downstream raw materials:

N,N'-(4,8-dinitro-9,10-dioxo-9,10-dihydro-anthracene-1,5-diyl)-bis-oxalamic acid

1,4,5,8-tetraaminoanthraquinone