Carbonic acid, (4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10 -bis[(trimethylsilyl)oxy]-1,4-ethanonaphthacen-5-yl ester

Base Information

Chemical Name:Carbonic acid, (4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10 -bis[(trimethylsilyl)oxy]-1,4-ethanonaphthacen-5-yl ester
CAS No.:74827-82-0
Molecular Formula:C35H41NO11Si2
Molecular Weight:707.882
Hs Code.:

Carbonic acid, (4-nitrophenyl)methyl
1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10
-bis[(trimethylsilyl)oxy]-1,4-ethanonaphthacen-5-yl ester

Synonyms:

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Chemical Property of Carbonic acid, (4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10 -bis[(trimethylsilyl)oxy]-1,4-ethanonaphthacen-5-yl ester

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Technology Process of Carbonic acid, (4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10 -bis[(trimethylsilyl)oxy]-1,4-ethanonaphthacen-5-yl ester

There total 6 articles about Carbonic acid, (4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10 -bis[(trimethylsilyl)oxy]-1,4-ethanonaphthacen-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2161-90-2
1-methoxy-1,3-cyclohexadiene

: 74827-82-0
(4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10-bis(trimethylsilyloxy)-1,4-ethanonaphthacen-5-yl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 20 °C

2: KH, PbO₂ / tetrahydrofuran

3: CH₂Cl₂ / 48 h / 25 °C

With potassium hydride; lead dioxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00538a081

Reference yield:

: 74827-78-4
p-nitrocarbobenzoxy naphthazarin

: 74827-82-0
(4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10-bis(trimethylsilyloxy)-1,4-ethanonaphthacen-5-yl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 20 °C

2: KH, PbO₂ / tetrahydrofuran

3: CH₂Cl₂ / 48 h / 25 °C

With potassium hydride; lead dioxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00538a081

Reference yield:

: 74827-79-5
1,4,4a,9,9a,10-hexahydro-8-hydroxy-1-methoxy-9,10-dioxo-1,4-ethanoanthracen-5-yl(4-nitrophenyl)methyl carbonate

: 74827-82-0
(4-nitrophenyl)methyl 1,4,6,6a,7,10,10a,11-octahydro-12-hydroxy-1-methoxy-6,11-dioxo-8,10-bis(trimethylsilyloxy)-1,4-ethanonaphthacen-5-yl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: KH, PbO₂ / tetrahydrofuran

2: CH₂Cl₂ / 48 h / 25 °C

With potassium hydride; lead dioxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00538a081