O-(2,6-Dichloro-4-nitrophenyl) dimethylcarbamothioate

Base Information

Chemical Name:O-(2,6-Dichloro-4-nitrophenyl) dimethylcarbamothioate
CAS No.:74875-14-2
Molecular Formula:C9H8Cl2N2O3S
Molecular Weight:295.146
Hs Code.:
DSSTox Substance ID:DTXSID30506045
Wikidata:Q82361599

Synonyms:74875-14-2;O-(2,6-Dichloro-4-nitrophenyl) dimethylcarbamothioate;SCHEMBL2924577;DTXSID30506045;LGLZFHKCTJYNCK-UHFFFAOYSA-N;FT-0769210;Dimethyl-thiocarbamic acid O-(2,6-dichloro-4-nitro-phenyl)ester

Suppliers and Price of O-(2,6-Dichloro-4-nitrophenyl) dimethylcarbamothioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(2,6-Dichloro-4-nitrophenyl) dimethylcarbamothioate

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:293.9632687
Heavy Atom Count:17
Complexity:299

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C(=S)OC1=C(C=C(C=C1Cl)[N+](=O)[O-])Cl

Technology Process of O-(2,6-Dichloro-4-nitrophenyl) dimethylcarbamothioate

There total 1 articles about O-(2,6-Dichloro-4-nitrophenyl) dimethylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 618-80-4
2,6-dichloro-4-nitrophenol

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

: 74875-14-2
O-(2,6-dichloro-4-nitrophenyl) dimethylcarbamothioate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In N,N-dimethyl-formamide; at 25 ℃; for 18h;

Reference yield:

: 74875-14-2
O-(2,6-dichloro-4-nitrophenyl) dimethylcarbamothioate

: 74875-15-3
S-(2,6-dichloro-4-nitrophenyl) dimethylcarbamothioate

Guidance literature:: at 175 - 180 ℃; for 0.166667h;
DOI:10.1021/jm00184a005

Reference yield:

: 74875-14-2
O-(2,6-dichloro-4-nitrophenyl) dimethylcarbamothioate

: 920509-81-5
4-amino-2,6-dichlorobenzenethiol

Guidance literature:: Multi-step reaction with 3 steps

1: 4 h / 200 °C

2: iron; acetic acid / water; isopropyl alcohol / 2 h / 95 °C

3: potassium hydroxide; water / ethanol / 16 h / 100 °C

With water; iron; acetic acid; potassium hydroxide; In ethanol; water; isopropyl alcohol;