N,4-Dimethyl-N-(trimethylsilyl)benzene-1-sulfonamide

Base Information

Chemical Name:N,4-Dimethyl-N-(trimethylsilyl)benzene-1-sulfonamide
CAS No.:74948-31-5
Molecular Formula:C₁₁H₁₉NO₂SSi
Molecular Weight:257.429
Hs Code.:
DSSTox Substance ID:DTXSID40503126
Wikidata:Q82356680

Synonyms:74948-31-5;N,4-Dimethyl-N-(trimethylsilyl)benzene-1-sulfonamide;DTXSID40503126;N,4-DIMETHYL-N-(TRIMETHYLSILYL)BENZENESULFONAMIDE

Suppliers and Price of N,4-Dimethyl-N-(trimethylsilyl)benzene-1-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,4-Dimethyl-N-(trimethylsilyl)benzene-1-sulfonamide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:257.09057656
Heavy Atom Count:16
Complexity:321

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N(C)[Si](C)(C)C

Technology Process of N,4-Dimethyl-N-(trimethylsilyl)benzene-1-sulfonamide

There total 1 articles about N,4-Dimethyl-N-(trimethylsilyl)benzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21149-38-2
2,2,2-trifluoro-N,N-bis(trimethylsilyl)-acetamide

: 640-61-9
N-methyl-p-toluenesulfonylamide

: 74948-31-5
N-methyl-N-trimethylsilyl-p-tolylsulfonamide

Guidance literature:: In acetonitrile; for 3h; Heating;
DOI:10.1039/P29840000077

Reference yield:

: 1730-69-4
dibutylchloroborane

: 74948-31-5
N-methyl-N-trimethylsilyl-p-tolylsulfonamide

: 74941-40-5
CH₃C₆H₄SO₂N(CH₃)B(C₄H₉)2

Guidance literature:: In neat (no solvent); byproducts: (CH3)3SiCl; (N2); to sulfonamidederiv. was slowly dropped boranederiv. and mixt. was slowly heated to 130°C and kept for 30 min at the same temp.; solvent and silanederiv. were removed in vac. and residue distd. in vac.; elem. anal.;
DOI:10.1016/S0022-328X(00)83053-3

Reference yield:

: 3677-81-4
diphenylboronchloride

: 74948-31-5
N-methyl-N-trimethylsilyl-p-tolylsulfonamide

: 74941-41-6
CH₃C₆H₄SO₂N(CH₃)B(C₆H₅)2

Guidance literature:: In neat (no solvent); byproducts: (CH3)3SiCl; (N2); to sulfonamidederiv. was slowly dropped boranederiv. and mixt. was slowly heated to 130°C and kept for 30 min at the same temp.; solvent and silanederiv. were removed in vac. and residue sublimated invac.; elem. anal.;
DOI:10.1016/S0022-328X(00)83053-3