Oxiranemethanol, 2,3-diphenyl-, (2S,3S)-

Base Information

Chemical Name:Oxiranemethanol, 2,3-diphenyl-, (2S,3S)-
CAS No.:74963-01-2
Molecular Formula:C15H14O2
Molecular Weight:226.275
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Oxiranemethanol, 2,3-diphenyl-, (2S,3S)-

Chemical Property:

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Technology Process of Oxiranemethanol, 2,3-diphenyl-, (2S,3S)-

There total 13 articles about Oxiranemethanol, 2,3-diphenyl-, (2S,3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1504-52-5
2,3-diphenyl-2-propen-1-ol

: 74963-01-2
((2S,3S)-2,3-diphenyloxiran-2-yl)methanol

Guidance literature:: 2,3-diphenyl-2-propen-1-ol; With oxovanadium(IV) sulfate; N-hydroxy-N-((1R,2R)-2-(4-methylphenylsulfonamido)cyclohexyl)-2,2-diphenylacetamide; In water; toluene; at 20 ℃; for 0.5h;

With tert.-butylhydroperoxide; In water; toluene; at 0 ℃; for 48h; optical yield given as %ee;
DOI:10.1021/jo900294h

Reference yield: 88.0%

: 22835-64-9
α-phenylcinnamyl alcohol

: 74963-01-2,78419-62-2,88424-61-7
(2RS,3RS)-2,3-epoxy-2,3-diphenyl-propan-1-ol

Guidance literature:: With tert.-butylhydroperoxide; (1S,4R)-N-(1-adamantyl)-N-hydroxy-2-oxobornan-10-amide; vanadium(V) oxytriisopropoxide; In decane; at 0 ℃; for 4h;
DOI:10.1016/S0957-4166(02)00741-3

Reference yield:

: 22835-64-9
α-phenylcinnamyl alcohol

: 74963-01-2
((2S,3S)-2,3-diphenyloxiran-2-yl)methanol

: 88424-61-7
((2R,3R)-2,3-diphenyloxiran-2-yl)methanol

Guidance literature:: With trityl hydroperoxide; (S)-N-diphenylmethyl-N-hydroxy-1-(2-methoxynaphthalen-1-yl)naphthalene-2-carboxamide; vanadium(V) oxytriisopropoxide; In toluene; at -20 ℃; for 68h; Product distribution; other reagents (S)-N-benzyl-N-hydroxy-1-(2-methoxynaphthalen-1-yl)naphthalene-2-carboxamide; (S)-N-cyclohexyl-N-hydroxy-1-(2-methoxynaphthalen-1-yl)napthalene-2-carboxamide;
DOI:10.1021/jo9821933