(E)-1,2-Diphenylpropene-3-ol

Base Information

Chemical Name:(E)-1,2-Diphenylpropene-3-ol
CAS No.:22835-64-9
Molecular Formula:C15H14 O
Molecular Weight:210.276
Hs Code.:
NSC Number:167101
Nikkaji Number:J834.404C,J953.645K
Mol file:22835-64-9.mol

Synonyms:22835-64-9;SCHEMBL3577072;SCHEMBL3577074;2,3-Diphenyl-2-propene-1-ol;(E)-1,2-Diphenylpropene-3-ol;NSC167101;NSC-167101

Suppliers and Price of (E)-1,2-Diphenylpropene-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (E)-1,2-Diphenylpropene-3-ol

Chemical Property:

Vapor Pressure:1.47E-05mmHg at 25°C
Boiling Point:351.9°Cat760mmHg
Flash Point:150.8°C
Density:1.106g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:210.104465066
Heavy Atom Count:16
Complexity:220

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=C(CO)C2=CC=CC=C2
Isomeric SMILES:C1=CC=C(C=C1)/C=C(/CO)\C2=CC=CC=C2

Technology Process of (E)-1,2-Diphenylpropene-3-ol

There total 19 articles about (E)-1,2-Diphenylpropene-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 13702-35-7,1755-47-1
(E)-2,3-diphenyl-propenal

: 22835-64-9
α-phenylcinnamyl alcohol

Guidance literature:: With sodium tetrahydroborate; In methanol; for 4h; Ambient temperature;
DOI:10.1055/s-1987-28142

Reference yield: 89.0%

: 124-38-9,18923-20-1
carbon dioxide

: 501-65-5
diphenyl acetylene

: 22835-64-9
α-phenylcinnamyl alcohol

Guidance literature:: With Triethoxysilane; ((4,4'-bi-1,3-benzodioxole)-5,5'-diyl)bis(bis(3,5-di-tert-butylphenyl)phosphine); cesium acetate; copper diacetate; In cyclohexane; at 60 ℃; for 25h; under 760.051 Torr; Reagent/catalyst; Solvent; Catalytic behavior; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202012768

Reference yield: 87.0%

: 64-18-6
formic acid

: 501-65-5
diphenyl acetylene

: 22835-64-9
α-phenylcinnamyl alcohol

Guidance literature:: diphenyl acetylene; With cesium acetate; copper diacetate; [(4S)-4-[5-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphanyl-1,3-benzodioxol-4-yl]-4,5,6,7-tetrahydro-1,3-benzodioxol-5-yl]-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphane; In cyclohexane; for 0.5h; Glovebox; Schlenk technique; Inert atmosphere;

formic acid; With Triethoxysilane; In cyclohexane; at 55 ℃; for 24h; Inert atmosphere; Sealed tube; Schlenk technique;

With ammonium fluoride; In methanol; at 20 ℃; for 0.25h; Reagent/catalyst; Solvent; stereoselective reaction; Catalytic behavior; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.1c01473