Tellurophene, 2-(4-methoxyphenyl)-

Base Information

Chemical Name:Tellurophene, 2-(4-methoxyphenyl)-
CAS No.:75073-61-9
Molecular Formula:C11H10OTe
Molecular Weight:285.8
Hs Code.:

Synonyms:

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Chemical Property of Tellurophene, 2-(4-methoxyphenyl)-

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Technology Process of Tellurophene, 2-(4-methoxyphenyl)-

There total 5 articles about Tellurophene, 2-(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 288-08-4
Tellurophen

: 696-62-8
para-iodoanisole

: 75073-61-9
2-(4-methoxyphenyl)tellurophene

Guidance literature:: Tellurophen; With tributyltin chloride; In diethyl ether; at 20 ℃; Inert atmosphere;

With n-butyllithium; In diethyl ether; hexane; at 20 ℃; for 0.75h;

para-iodoanisole; With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; In N,N-dimethyl-formamide; at 50 - 60 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1216958

Reference yield:

: 14063-79-7
3-chloro-3-(4-methoxyphenyl)acrylaldehyde

: 75073-61-9
2-(4-methoxyphenyl)tellurophene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Na2Te / 1.) DMF, 0 deg C, 1 h, then RT, 45 min, 2.) α-bromo-ethyl acetate, DMF, 0 deg C, 1.5 h, then RT, 1 h

2: 3.0 g / NaOH / ethanol; H₂O / 2.5 h / Heating

3: 1.9 g / copper chromite / quinoline / 3 h / Heating

With sodium hydroxide; disodium telluride; copper chromite; In quinoline; ethanol; water;

Reference yield:

: 2-(p-methoxyphenyl)-5-ethoxycarbonyltellurophen

: 75073-61-9
2-(4-methoxyphenyl)tellurophene

Guidance literature:: Multi-step reaction with 2 steps

1: 3.0 g / NaOH / ethanol; H₂O / 2.5 h / Heating

2: 1.9 g / copper chromite / quinoline / 3 h / Heating

With sodium hydroxide; copper chromite; In quinoline; ethanol; water;