1,4-Disilacyclohexa-2,5-diene, 1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl-

Base Information

Chemical Name:1,4-Disilacyclohexa-2,5-diene, 1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl-
CAS No.:751-37-1
Molecular Formula:C32H32Si2
Molecular Weight:472.777
Hs Code.:
DSSTox Substance ID:DTXSID00499450
Nikkaji Number:J1.984.971F
Wikidata:Q82350231

Synonyms:751-37-1;1,4-Disilacyclohexa-2,5-diene, 1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl-;1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl-1,4-disiline;DTXSID00499450;1,1,4,4-Tetramethyl-2,3,5,6-tetraphenyl-1,4-dihydro-1,4-disiline

Suppliers and Price of 1,4-Disilacyclohexa-2,5-diene, 1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,4-Disilacyclohexa-2,5-diene, 1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl-

Chemical Property:

PSA：0.00000
LogP:8.79560
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:472.20425409
Heavy Atom Count:34
Complexity:635

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si]1(C(=C([Si](C(=C1C2=CC=CC=C2)C3=CC=CC=C3)(C)C)C4=CC=CC=C4)C5=CC=CC=C5)C

Technology Process of 1,4-Disilacyclohexa-2,5-diene, 1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl-

There total 6 articles about 1,4-Disilacyclohexa-2,5-diene, 1,1,4,4-tetramethyl-2,3,5,6-tetraphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 86840-61-1
13,13-Dimethyl-1,10-diphenyl-13-silatricyclo<8.2.1.0^Δ2,9>trideca-11-en

: 501-65-5
diphenyl acetylene

: 751-37-1
2,3,5,6-tetraphenyl-1,1,4,4-tetramethyl-1,4-disila-2,5-cyclohexadiene

Guidance literature:: at 200 ℃; for 2.5h;
DOI:10.1016/0022-328X(86)80390-4

Reference yield: 34.0%

: 4098-30-0
dodecamethylcyclohexasilane

: 501-65-5
diphenyl acetylene

: 751-37-1
2,3,5,6-tetraphenyl-1,1,4,4-tetramethyl-1,4-disila-2,5-cyclohexadiene

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1-adamantyl isocyanide; In toluene; at 100 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.organomet.8b00302