1,3-Benzodioxole, 2-phenyl-

Base Information

Chemical Name:1,3-Benzodioxole, 2-phenyl-
CAS No.:7527-52-8
Molecular Formula:C13H10O2
Molecular Weight:198.221
Hs Code.:
DSSTox Substance ID:DTXSID00452565
Nikkaji Number:J982.094I
Wikidata:Q82273277

Synonyms:1,3-Benzodioxole, 2-phenyl-;2-phenyl-benzodioxole;7527-52-8;SCHEMBL3766975;DTXSID00452565

Suppliers and Price of 1,3-Benzodioxole, 2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1,3-Benzodioxole, 2-phenyl-

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:198.068079557
Heavy Atom Count:15
Complexity:197

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2OC3=CC=CC=C3O2

Technology Process of 1,3-Benzodioxole, 2-phenyl-

There total 7 articles about 1,3-Benzodioxole, 2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.2%

: 100-52-7
benzaldehyde

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 7527-52-8
2-phenyl-1,3-benzodioxole

Guidance literature:: With Cu(II) impregnated sulfated MCM-41; In toluene; benzene; for 0.5h; Reflux;
DOI:10.1080/15533174.2010.538018

Reference yield: 53.0%

: 274-09-9
Methylenedioxybenzene

: 98-80-6
phenylboronic acid

: 7527-52-8
2-phenyl-1,3-benzodioxole

Guidance literature:: Methylenedioxybenzene; phenylboronic acid; With bis(acetylacetonate)nickel(II); potassium phosphate; triphenylphosphine; for 0.0833333h; Inert atmosphere; Schlenk technique;

With di-tert-butyl peroxide; at 100 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201300459