2-Methyl-1-phenylpent-1-en-3-one

Base Information

Chemical Name:2-Methyl-1-phenylpent-1-en-3-one
CAS No.:75391-07-0
Molecular Formula:C12H14O
Molecular Weight:174.243
Hs Code.:
DSSTox Substance ID:DTXSID20396018

Synonyms:2-methyl-1-phenylpent-1-en-3-one;75391-07-0;DTXSID20396018;2-Methyl-1-phenyl-1-penten-3-on

Suppliers and Price of 2-Methyl-1-phenylpent-1-en-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-1-phenylpent-1-en-3-one

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:174.104465066
Heavy Atom Count:13
Complexity:197

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=O)C(=CC1=CC=CC=C1)C

Technology Process of 2-Methyl-1-phenylpent-1-en-3-one

There total 19 articles about 2-Methyl-1-phenylpent-1-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 599187-68-5
C₁₆H₂₁NO

: 925-90-6
ethylmagnesium bromide

: 75391-07-0,57558-68-6
2-methyl-1-phenylpent-1-en-3-one

Guidance literature:: C₁₆H₂₁NO; With 2-fluoropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

ethylmagnesium bromide; In dichloromethane; at -78 ℃; for 0.416667h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; dichloromethane; at 65 ℃; for 2h; chemoselective reaction; Inert atmosphere;
DOI:10.1038/nchem.1268

Reference yield: 92.0%

: 100-52-7
benzaldehyde

: 96-22-0
pentan-3-one

: 75391-07-0
(E)-2-methyl-1-phenyl-1-pentene-3-one

Guidance literature:: With hexan-1-amine; 6-cyclohexyl-12-fluoro-5,6,7,12-tetrahydrodibenzo[c,f ][1,5]azastibocine; In water; at 20 ℃; for 4h; diastereoselective reaction; Schlenk technique;
DOI:10.1039/c9dt01100e