4-Chloro-2-(2-methylanilino)benzohydrazide

Base Information

Chemical Name:4-Chloro-2-(2-methylanilino)benzohydrazide
CAS No.:75412-39-4
Molecular Formula:C₁₄H₁₄ClN₃O
Molecular Weight:275.738
Hs Code.:
DSSTox Substance ID:DTXSID40503924
Wikidata:Q82358046

Synonyms:4-Chloro-2-(2-methylanilino)benzohydrazide;75412-39-4;DTXSID40503924

Suppliers and Price of 4-Chloro-2-(2-methylanilino)benzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-Chloro-2-(2-methylanilino)benzohydrazide

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:275.0825398
Heavy Atom Count:19
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1NC2=C(C=CC(=C2)Cl)C(=O)NN

Technology Process of 4-Chloro-2-(2-methylanilino)benzohydrazide

There total 4 articles about 4-Chloro-2-(2-methylanilino)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77817-51-7
4-Chloro-2-o-tolylamino-benzoic acid methyl ester

: 75412-39-4
4-Chloro-2-o-tolylamino-benzoic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 16h; Yield given; Heating;

Reference yield:

: 50-84-0
2,4 dichlorobenzoic acid

: 75412-39-4
4-Chloro-2-o-tolylamino-benzoic acid hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃, copper powder / pentan-1-ol

2: SOCl₂ / 12 h / Heating

3: hydrazine hydrate / ethanol / 16 h / Heating

With thionyl chloride; copper; potassium carbonate; hydrazine hydrate; In ethanol; pentan-1-ol;

Reference yield:

: 32305-28-5
4-chloro-2-o-toluidino-benzoic acid

: 75412-39-4
4-Chloro-2-o-tolylamino-benzoic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 12 h / Heating

2: hydrazine hydrate / ethanol / 16 h / Heating

With thionyl chloride; hydrazine hydrate; In ethanol;