Diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate

Base Information

Chemical Name:Diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate
CAS No.:75628-82-9
Molecular Formula:C24H20O4
Molecular Weight:372.42
Hs Code.:
DSSTox Substance ID:DTXSID70503937
Nikkaji Number:J1.412.362H

Synonyms:75628-82-9;Diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate;DTXSID70503937

Suppliers and Price of Diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate

Chemical Property:

XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:372.13615911
Heavy Atom Count:28
Complexity:573

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC(=C2C1=CC=C(C=C2)C#CC3=CC=CC=C3)C(=O)OCC

Technology Process of Diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate

There total 2 articles about Diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1157-45-5
diethyl 6-bromoazulene-1,3-dicarboxylate

: 536-74-3
phenylacetylene

: 75628-82-9
diethyl 6-(phenylethynyl)azulene-1,3-dicarboxylate

Guidance literature:: With copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; In toluene; at 20 ℃; for 9h;
DOI:10.1016/S0040-4039(00)01445-3