1H-Benzimidazol-2-amine, N-methyl-N-4-piperidinyl-, dihydrobromide

Base Information

Chemical Name:1H-Benzimidazol-2-amine, N-methyl-N-4-piperidinyl-, dihydrobromide
CAS No.:75970-60-4
Molecular Formula:C13H18N4.2BrH
Molecular Weight:392.137
Hs Code.:

Synonyms:

Suppliers and Price of 1H-Benzimidazol-2-amine, N-methyl-N-4-piperidinyl-, dihydrobromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1H-Benzimidazol-2-amine, N-methyl-N-4-piperidinyl-, dihydrobromide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Benzimidazol-2-amine, N-methyl-N-4-piperidinyl-, dihydrobromide

There total 6 articles about 1H-Benzimidazol-2-amine, N-methyl-N-4-piperidinyl-, dihydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 98245-13-7
ethyl 4-<(1H-benzimidazol-2-yl)methylamino>-1-piperidinecarboxylate

: 75970-60-4
N-methyl-N-(4-piperidinyl)-1H-benzimidazol-2-amine dihydrobromide

Guidance literature:: With hydrogen bromide; at 120 ℃; for 2h;
DOI:10.1021/jm00150a029

Reference yield:

: 2719-30-4
o-nitrophenylisothiocyanate

: 75970-60-4
N-methyl-N-(4-piperidinyl)-1H-benzimidazol-2-amine dihydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / ethanol / Ambient temperature

2: 95 percent / H₂, ammonia / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

3: 84 percent / yellow HgO, sulfur / methanol / 2 h / Heating

4: 95 percent / 48 percent aq. hydrobromic acid / 2 h / 120 °C

With ammonia; hydrogen bromide; hydrogen; sulfur; mercury(II) oxide; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00150a029

Reference yield:

: 73733-69-4
ethyl 4-(methylamino)piperidine-1-carboxylate

: 75970-60-4
N-methyl-N-(4-piperidinyl)-1H-benzimidazol-2-amine dihydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / ethanol / Ambient temperature

2: 95 percent / H₂, ammonia / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature

3: 84 percent / yellow HgO, sulfur / methanol / 2 h / Heating

4: 95 percent / 48 percent aq. hydrobromic acid / 2 h / 120 °C

With ammonia; hydrogen bromide; hydrogen; sulfur; mercury(II) oxide; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00150a029